GCMS analysis results for sample AD30633, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : M:\lNSTRU~l\209\DATA\DEC2701\30633.D Vial: 27 Acq On : 28 Dec 2001 3:23 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.62 3.90 ug/1 1314680 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 1,3 -Dioxolane, 2 -pentadecyl - 284 C18H3602 004360-57-0 9 4 Silane, tetramethyl-_________________ 88 C4H12Si 000075-76-3 9 Abundance < Scan 280 (7.618 min): 30633.D (-) m/z 73.00 100.00% 73

5000 43

L 187 103 7.20 7.40 7.60 m/z 43.00 7.80 8.00 30.64% m/z—> 20 40 60 80 100 120 140 -160 180' '266' 220 240 260 280 Abundance #292: N-Ethylformamide 30 73

5000 44 58 7.20 7.40 7.60 7.80 8.00 m/z 41.00 11.25% 15 it । , 1 ‘ i ■ ■ ■ ■ iI ' ■ ■ ■ i ■ ■ • ■ । ■ i > • । । । । ■ • ■ ■ । •■ht 111 ■ 111 ■ 111111 > 11 > ■ ■ r ■ > 111 ■ । miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #62902: 1.3-Dioxolane, 2-methyl- 73 —TPrTmmrrfrmm 7.20 7.40 7.60 7.80 8.00 5000 43 m/z 45.05 11.20% ' 58 27 i ( 87 ■ ‘ I ' ‘' . 11. । > >. 11.11, ।। ।।111111111111111111 ri 111111111 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #40191: 1,3-Dioxolane, 2-pentadecyl- mmmmTTTm 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.75% 5000

43 57 86 99 256 283 m/z-> 20 40 60 80 100 126' ‘146' 160 iso 266' 226' 246' 260 280' 7.20 1-17.40 r' 7.60 ' 7.80 8.00 '

30633.D GCMS0103.M Thu Jan 10 15:23:22 2002 Page 1

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