GCMS analysis results for sample AD29671, Jan 2002

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Library Search Compound Report

Data File : M:\INSTRU~1\2O9\DATA\DEC13O1\29671.D Vial: 18 Acq On : 14 Dec 2001 1:29 am Operator: 209 GALOS Sample • : gems scan 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.59 2.98 ug/1 1058330 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformami e 73 C3H7NO 000627-45-2 9 2 1,3 -Dioxolane, 2- (3-bromo-5, 5, 5-tri 352 C10H16BrC13O2 000000-00-0 9 3 3-Pentanol, /3-methyl- 102 C6H140 000077-74-7 9 4 Silane, tet ramethyl- 88 C4H12Si 000075-76-3 9 Abundance 7 Scan 277 (7,590 min): 29671.D (-) m/z 72.95 100.00% 73

5000- 43 '-|-| - i 7.20 7.40 7.60 7.80 8.00 3x ' 1 1 1 1 1 ' I 1 ' 1 1 1...........1111 1 1 55 50 67, 1 ' 1 I ' 1 1 'I' 4t 87 103 m/z 43.05 26.71% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 'Abundance #292: N-Ethylformamide 30 a 73

5000 - 58 7.20 7.40 7.60 7.80 8.00 44 m/z 44.95 9.69% 1541 '4014 — m/z—> 1G 20 30 50 60 70 80 90 100 110 120 Abundance #49423: 1.3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet 73 । ■ ■ > ■ । ■ 1 1 ■ i ■ ■ 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.05 9.65% 45 36 55 67 , 109,115 1 i ■ ■ ' ■ i ' ■ ■'i '1 '■ i • 1■ 1 i ■ ■ ' ■ i ■ ■ ■ 'i ■ ■ ■ ' i ■ '

m/z-> 10__ 20 30 40 50 60 70 80 90 100 110 120 — Abundance #63573: 3-Pentanol, 3-methyl- T r1 1 TT—TrTr 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.00 6.25% 5000 55 ,7 45 87 r, । .... । r. , , । 1 , 39, 1 . .j . । । । । 1 --- s । । — P r T TTT TIPT —I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00

29671.D GCMS1126.M Tue Jan 08 11:02:55 2002 Page 1

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