GCMS analysis results for sample AD29734, Jan 2002

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Library Search Compound Report

Data File : M:\INSTRU~l\209\DATA\DEC1301\29734.D Vial: 20 Acq On : 14 Dec 2001 3:26 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K. L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.59 2.64 ug/1 935307 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 000627-45-2 9 73 C3H7NO 2 Silane, tetramethyl - 000075-76-3 9 88 C4H12Si 3 1,3-Dioxola 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 Abundance / Scan 278 (7.594 min): 29734.D (-) m/ z 73.00 100.00% ! 73

5000 43 .............. 1 87 103 7.20 7.40 7.60 7.80 8.00 : 0 — | —PPP 1 381 149 55 1 I ' ' 67, , ' ■ • Pm — I m/ z 43.05 27.22% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide

73

5000- 44 58 7.20 7.40 7.60 7.80 8.00 m/z 44.95 10.21% 15 J 4 50 m/z-> 10 20 30 40 60 70 80 90 100 110 120 Abundance #62932: Silane, tetramethyl- 73 , T——TTTTTTTT I 7.20 7.40 7.60 7.80 8.00 5000- m/z 41.05 9.80% 45 15 53 59 88 1 ' । ' 11 ' I ' ' ' ' i ■ ■ ■ ■ i 1 1 ■ ' i 1 ' ■ ■ i ■ ' ' ' i ■ ■ ■ ■ i • ■ • ' i ■ ■ ■ ■ i 1 1 1 1 I 1 1 1 ' I 1 1 m/z-> Abundance 10 20__ 30 40 50 60 70 80 #49423: 1,3-Dioxolane. 2-(3-bromo-5,5,5-trichloro-2,2-dimet 73 90 100 110 120 - L= — 7.20 7.40 7.60 7.80 8.00 m/z 71.0,0 6.31% 5000 45

1 361 55 ■ ■ i ■ ■ • ' i > • > ■ i ■ • ; ■ । ■ ■ • > । > < । i 67, +r ................................. 1,09 115 । —IT——n—T m/z-> 10 20 30 40 50 . 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00

29734.D GCMS1126.M Tue Jan 08 11:04:17 2002 Page 1

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