GCMS calibration table for TCLP method, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : M:\INSTRU~1\209\DATA\DEC1301\29522 .D Vial: 21 Acq On : 14 Dec 2001 4:25 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

7.59 2.47 ug/1 922644 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 entative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Pentane/ 3-methoxy- 102 C6H140 036839-67-5 9 3 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 Silane, tetramethyl- 88 C4H12S1 000075-76-3 7 Abundance Scan 278 (7.594 min): 29522.D (-) m/ z 73.00 100.00%! 73

5000 43 I 1....... 87 ..........103................ 7.20 7.40 7.60 7.80 8.00

m/z—> P ' ' ' i ■ ' ' ' i ■ 10 20 30 38■I. 1 49 55 I 1 11 1 I TTIUT 40 50 60 70 80 67— 90 100 110 120 m/ z 43.00 27.60% Abundance #292: N-Ethylformamide 30 73

5000 1 TTT ' 1 i ■ ■ 58 7.20 7.40 7.60 7.80 8.00 44 m/z 41.05 10.26%

m/z-> 410 20 30 — 40 50 60 70 p ■ ' ■ । ■ ■ ■ ■ । ' 80 90 100 110 120 Abundance #1793: Pentane. 3-methoxy- 73 10—————— rT 7.20 7.40 7.60 7.80 8.00 5000- m/ z 45.05 9.67% 45

27 33 39 55 Id—nmau————mun—puuir TT । i i r-i-]-i 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane. 2-(3-bromo-5,5,5-trichloro-2,2-dimet ------- 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.23% 5000

45 .................................. 36 It 55 67. ' i ■ ■ ■ ' i ■ ■ ■ ■ i ' ' 1 ■ i ■ 1 I ' ' 1 1 ' ‘ 1 I 1 _ 109,115, m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 7.40 7.60 7.80 8.00

29522.D GCMS1126.M Tue Jan 08 10:53:46 2002 Page 1

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