Quality reviewed GCMS calibration data listing surrogate compounds and retention times from December 14, 2001.
NYC-WTC_000036729–000036751Folder label: “GCMS X 12/7/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\INSTRU~1\209\DATA\DEC1301\29522.D Vial: 21 Acq On : 14 Dec 2001 4:25 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Platinum, bis [ (1,2,5,6-.eta.)- Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
11.84 12.12 ug/1 4525060 1,4-Dichlorobenzene-d4 11.67
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Platinum, bis11,2,5,6-.eta.)-1,5-c 411 C16H24Pt 012130-66-4 59 2 1,5-Cyclooctadiene, (E,Z)- 108 C8H12 005259-71-2 59 3 Cyclohexend, 4-ethenyl- 108 C8H12 000100-40-3 47 4 1,5-Cyclooctadiene, (Z,Z)~ 108 C8H12 _________ 001552-12-1 40 Abundance Scan 740 (11.835 min): 29522.D (4 m/z 54.00 100.00% 1 54
80 107 5000
m/z-> 0 ask—. TIT I‘‘TT‘TTTTTTTTTTTTT I I I I I I M t I | . < I I p < I . | I I I I | . I H t I . I I ! I I I . | I I I I | I 20 40 60 80 100120140 160 180 200 220 240 260 280 300 320 340 360 380 400 m/z 11.60 11.80 12.00 12.20 80.00 54.41% Abundance #54668: Platinum, bis[(1,2,5,6-.eta.)-1,5-cyclooctadiene]- 54
- 5000 80 27 11.601 11.80 12.00 12.20 m/z 79.05 53.94%
m/z-> TT I' I" " I 118 411 11"111 r*1 IET’TTEEEIIETTITTTTEETTTTTTTUUTCUTIUTTT’TTTTI’TT 20 40 60 80 100120140160180200220 240260 280 300 320 340 360 380 400 303
Abundance #2170: 1.5-Cyclooctadiene, (E.Z)- 54 1 1 I ’ 1 11.60 11.80 12.00 12.20 5000 ' 79 m/z 107.00 50.99%
//i 108 __________ ______________ ‘I‘EETIEu"EEETEETTTTETOETT ___ ‘EO‘TEIGTTOOTTTTTUTTITTTTT I' ■ ■' I " ■' I ■ • ■ - j ■ *»■ I ‘'’ I • ■' ■ 11 • • 11' m/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance। #63795: Cyclohexene, 4-ethenyl- 54 11.60 11.80 12.00 12.20 m/z 41.00 50.89% 79 5000 27
miz-> 1 I .1 108 TTTTTTT’TT’T’ T’TTTTETTTTEE’ETIII’IT I’E’IUETTTTETTEETITTII ’TT TT 1 1 I ' TTTT 20 40 60 80 100120 140 160180 200 220 240 260 280 300 320 340 360 380 400 11.60 11.80 12.00 12.20
29522.D GCMS1126.M Tue Jan 08 10:53:51 2002 Page 2
NYC-WTC_000036735
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NYC-WTC_000036752
Quality reviewed GCMS data listing surrogate compounds and retention times from January 3, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017630
Laboratory report documenting GCMS analysis of sample AD31023 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017595
Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017556
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31019 performed on January 18, 2002.
1 shared topics · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017542
Laboratory report documenting GCMS blank analysis for volatile organic compounds on sample AD30605 conducted on January 10, 2002.
1 shared topics · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.985
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017210
Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018005
Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000036689
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036690
Laboratory results for GCMS blank analysis of sample AD29522 showing detection levels below method detection limits.
Filed in the same folder
NYC-WTC_000036695
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036703
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036704
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder