GCMS results for unknowns, sample AD26827, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\26827.D Vial: 11 Acq On : 27 Dec 2001 9:53 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

11.13 0.31 ug/1 101435 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane octamethy1- 296 C8H24O4Si4 000556-67-2 86 2 Benzene, 1-phenyl/4-(2-cyano-2-phen 281 C21H15N 027869-56-3 53 3 2-Oxo-4-phenyl-6- (4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 4 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 Abundance Scan 663 (11,128 min): 26827.D (-) m/z 281.00 100.00% 281

5000

T T T T T 45 59 73 88 103 119 133 147 163 177 113 297 235 24% 225 10.80 11.00 11.20 11.40 Tri f > l > I p i't i“| FTTrt’t i i । V i i ′ i "T"i |fi i । i i i'i i .... । A . > |' ■ 'i ■’ ■' • i ■ • m/z 282.00 29.40% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

5000 T T 10.80 .11.00 11.20 11.40 X T

207 rn/z 283.00 17.35% 133

miz-> •»i • 40 73 i I 163 177 191 X , . 235 h I ■ ‘■ i ' ■' ■ i1 ■ ■ • > ■ • ■ ■ i • • ' ■ i 1 ■ ■ ■ i ■ • ■ ' i 60 80 100 120 140 160 180 200 220 240 265.. l, 260 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethery!) 281 ■ ■ i ■ ■ ■ ■ i ■ ■ • • i ■ • ■ ■ । 1 1 ■ ■ i 10.80 11.00 11.20 11.40 5000 m/z 192.90 13.47% 203 253 266 126 .............................................. T‘1B32/‘t0/‘32/02/0/2/0‘1t‘11/‘1102210922111211111111911110 —33113T T T1r 224240,"? m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyriml T T T T T 281 10.80 11.00 11.20 11.40 m/z 73.00 12.89% 5000

m/z-> 102 123 141 175 204 • ■ i • ■ ■ । L’Tr 11 > 111 j'i ri 11 ■! 11 ■ i 1 ■ ■ ■ i • ■' ■ i ■ ■ ■ • I hir 40 60 80 100 120 140 160 180 200 247......... 1 220 240 260 280 0 .................... ............................ 10.80 11.00 11.20 11.40

26827.D GCMS1126.M Tue Jan 29 14:24:52 2002 Page 3

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