GCMS results for unknowns, sample AD26477, Dec 2001

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GCMS analysis report for sample AD26477 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.

NYC-WTC_000018923–000018933

Folder label: “GCMS X 12/17/01 A 12/22 - 12/23/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\26477.D Vial: 10 Acq On : 27 Dec 2001 8:54 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ****************************************************************** *** Peak Number 2 Benzene, l-phenyl-4-(2-cyano-2 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.13 0.30 ug/1 92753 1,4-Dichlorobenzene-d4 11.68 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzene, 1-phenyl-4- (2-cyano-2-phen 281 C21H15N 027869-56-3 50 2 Cyclotetrasiloxane, octamethyl- 296 C8H24O4S14 000556-67-2 38 3 2-Oxo-4-phenyl-6- (4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 4 6,7-Benzo/phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 Abundance Scan 663 (11.128 mln): 26477.D (-) m/z 281.00 100.00% 281

5000

r* * T T 45 59 73 88 103 119 133 165177 193 207 22 249 265 10.80 11.00 11.20 11.40 TTIm—trrmmn.tn5emmemmTT J***235 ’I*’it*I I., .. *. I r m/z 282.0,0 28.21% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-pheny1ethenyl) 281

5000 T T 1148/4 1 I 1 1 1 1 I 10.80 11.00 11.20 11.40 203 253 m/z 283.00 15.24% 126 266 . ,224.240.1 H . 4| I miz-> 40 60 ‘' 80 100 120 140 160 180 '200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

10.80 11,00 11.20 11.40 5000 m/z 192.9,0 12.19%

73 133 207 J 163 177 191 235 249 265 ! ■ ■ । ■ ■ ■ ■ । • ■ • ■ । ■ ■ ■ • । • — ■ i ■ ■ ■ ■ 14 i ■' ■ ■ i • • ■ ■ i ■ ■ •11'1 1' i । ■ । ■ ■ m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756:2-Oxo-4-phenyl-6-(4-chloropheny!)-1,2-dihydropyrimi ■ ' । ' ' ■ ■ i ■ ■ ■ • 1 1 1 1 1 1 1 ' 1 1 1 i 281 10.80 11.00 11.20 11.40 m/z 133.0,0 11.53% 5000

.......... 192 , 123,141, . ............................. 1 -r-ryr-r T-TTp-r-TT-p-r-r-r-j- m/z—> 40 do 80 166 126 140 160 180 200 220 240 260’280 10.80 11.00 11.20 11.40

26477.D GCMS1126.M Tue Jan 29 14:22:12 2002 Page 2

NYC-WTC_000018931

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