GCMS analysis results for sample AD30633, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\30633.D Vial: 27 Acq On : 28 Dec 2001 3:23 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 11.13 0.45 ug/1 153263 1,4-Dichlorobenzene-d4 11.68 Hit# Of 5 Tentative ID MW MolForm CAS# Qual I Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 56 2 Benzene, 1-phenyl-4- (2-cyano-2-phen 281 C21H15N 027869-56-3 53 3 4-Amino-5 - (4-acetyl phenylazo) benzof 281 C14H11N5O2 000000-00-0 28 4 2-Oxo-4-ph^yl-6-(4-chlorophenyl) -1 282 C16H11C1N2O 000000-00-0 9 Abundance Scan 663 (11.134 min): 30633.D (-) m/z 281.00 100.00% 281

5000

T T T T T 10,80 11.00 11.20 11,40 ., 45 .59 73 85 . 193 118, 123 147 163 179 13 297 235 Zh, 225 . Har m/z 282.00 27.74% mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72646: Cyclotetrasiloxane, octamethyl- 281

........ /........ 5000 10.80 11.00 1120 11.40 ' 1 m/z 283.00 17.34% 265 45 59 73 133 177 193 207 235 1. ' 1 i1 ' • ■ i ■ ■ ■ • i 1 ■ • ■ i ■ ' • ‘ i ' ■' ‘ i ■ ■ ■ ' i ■ ■ ■ ■ i ■ ■ ‘ 1 i ‘ ' i ■ • • 1 i ■ • •1 i ' ‘1 ■ i • • m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643; Benzene, 1-phenyl-4-(2-cyano-2-phenylethery!) 281 ‘ ‘ i ' ■ ■ ■ i ‘ ■ 1 1 I ' 1 ' l 10.80 11.00 11.20 11.40 5000 m/z 192.90 11.08%

203 253 126 , 266 224 240 ■ • । ■' ■ ■ । • • ■ • । ■ ■ • • । ■11 ■ • ■ ■ । ■11 ■ ■ ■ ■ । ■11111111111111 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 '280 Abundance #39574:4-Amlno-5-(4-acetylphenylazo)benzofurazan TT-j-r-T ' ' 1 1 ■ ’ • I 281 10.80 11.00 11.20 11.40 m/z 133.00 9.68% 5000 116 134 162 77 180 194 209 238 252 266 miz-> ■ ■ i ■ ■ ■ ■ i ■ ■ 40 60 i ■ ■ ■ ■ i ■' IIdgusspusuafaauyudavunsAyusSapovp "‘1′4′13" ‘ ' i ■ ■ ■ ' i 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40

30633.D GCMS0103.M Thu Jan 10 15:23:31 2002 Page 2

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