NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 23 pages
GCMS analysis results for sample AD30633, Jan 2002
Machine-extracted title · confidence 95%Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.
NYC-WTC_000017210–000017232Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : M:\lNSTRU~l\209\DATA\DEC2701\30633.D Vial: 27 Acq On : 28 Dec 2001 3:23 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 14.31 3.06 ug/1 1298100 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 Benzoic acid, 2, 6-bis [ (trimethylsil 370 C16H30O4Si3 003782-85-2 40 3 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H32O3Si3 068595-79-9 38 4 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 37 Abundance Scan 1009 (14.310 min): 30633.D (-) m/ z 73.00 100.. 00% i 73
5000 267 355
45 , 1 89 108 133 154 177193 _ 223 251 | 293 323339 h 14.00 14.20 14.40 14.60 2‘100011—210mumBma—ummnmaammgT . f.,.. । .. .. |T.. . Tj. ■ 111 m/z 267.0,0 37.33% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 ■ ■ ■ i ■ 1 1 ' i 1 1 rn 1 r 1 1 i 1 1 1 1 i 14.00 14.20 14.40 14.60 m/z 355.05 29.17% 191207 251 323339 miz-> 40 60 80 100 120 140 160 180 ‘260’ '226' 240 260 280 300 320 340 360 ’ Abundance #51296: Benzoic acid, 2.6-bis[(trimethy silyl )oxy]- trimet 73 355
14.00 14.20 14.40 14.60 5000 m/ z 356.0.5 10.45% 147 267 47 , 208 249 | 283 sy*sssyasdoattaayvvosuoAdogoAoAgAA8*AAdAS*S*ASSSFSSSTI ‘ I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl) 73 14.00 14.20 14.40 14.60 ' ‘ ‘ m/z 267.9,0 9.68% 5000 267 179 356 45 147 ............................................................................................................. A ............... ■ ■ । • ' • ■ i ■ ■ 11 i • • • ■ । 1 1 1 1 i m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ‘ 14.00 14.20 14.40 14.60
30633.D GCMS0103.M Thu Jan 10 15:23:40 2002 Page 3
NYC-WTC_000017219
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NYC-WTC_000017219Source: NYC Law Department, mirrored locally
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