NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 19 pages
GCMS analysis results, sample AD30602, January 2002
Machine-extracted title · confidence 85%Gas chromatography-mass spectrometry analysis report for sample AD30602 showing detection of 2,4-DDD and other unknown compounds, analyzed January 22, 2002.
NYC-WTC_000017246–000017264Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\30602.D Vial: 30 Acq On : 28 Dec 2001 6:18 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 14.31 1.44 ug/1 619244 Naphthalene-d8 15.28
Hit# of 5 entative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 38 3 Benzeneethanamine, N- [ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 4 Benzoi acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37 .Abundance Scan 1009 (14.311 min): 30602.D (-) m/ z 73.00 100.00% 73
5000 267 355 d** TIB 45 14.00 14.20 14.40 14.60 ( , 125 — ■ .99 154 .193,223 , odos* Fit —afi t293 i । >323 *tmn r i r । i i i 11 i i i i । i i i i । i i m/z 267.00 37.13% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 14.00 14.20 14'46 14.60 ' ‘ ' m/z 355.05 29.95%
m/z-> -2 50 160150266256 323, ■ 1 • •' ■ 1 i ■ ' 1 ' i ' 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 300 350 400 450 500 550 Abundance #49868: 3,4-Dihydroxybenzyl alcohol, tris(trimethylsily!)- 73
14.00 14.20 14.40 14.60 267 5000 179 m/z 356.05 10.75% 356 45 147 209237, 312 | • ■ i ‘ ' • i • ■ ■ ■ i ■ ■ • ■ i 1 ' ' • I • ■ ■ • i ■ 1 1 ' I 1 1 1 1 I 1 1 1 1 1 1 1 1‘* I 11 1 1 | 1 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-Kpentafluorophenyl)methylene] ’AI418*I’’I’IT--*E 73 355 14.00 14.20 14.40 14.60 m/z 267.90 10.33% 5000
45 | 208 251 281 386 458 548 / ______ —I* ■ ■ i ■ ■ ' ■ i • • ■ • i 1 • • ■ i ■ ■ ■ ■ ।■11 • ■ ■1111 •'111 ■ ■11 m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.00 14.20 14.40 14.60
30602.D GCMS0103.M Thu Jan 10 15:45:02 2002 Page 2
NYC-WTC_000017254
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NYC-WTC_000017254Source: NYC Law Department, mirrored locally
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Laboratory report of GCMS analysis for sample AD28860 conducted on December 16, 2001, showing compound identification.
1 shared topics · Same agency, volume and box · similarity 0.993
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