NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 19 pages
GCMS analysis results, sample AD30602, January 2002
Machine-extracted title · confidence 85%Gas chromatography-mass spectrometry analysis report for sample AD30602 showing detection of 2,4-DDD and other unknown compounds, analyzed January 22, 2002.
NYC-WTC_000017246–000017264Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
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NYC 9/11 Public Portal Document Library Search Compound Report
Data File : M:\lNSTRU~l\209\DATA\DEC2701\30602.D Vial: 30 Acq On : 28 Dec 2001 6:18 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2H-1,4-Benzodiazepin-2-one, 7- Concentration Rank 1
R.T. EstCono Area Relative to ISTD R.T.
17.45 3.96 ug/1.. 1698020 Naphthalene-d8 15.28
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 2H-1,4-Benz.odiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 2 1,1,1,5,7,7 7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 16 3 3-Trimeth; silyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 9 4 Pregnane/! ,20-dione, 11-[(trimethyl 462 C26H46N2O3Si 057305-27-8 9 Abundance Scan 1351 (17.451 mln): 30602.D (-) m/ z 73.00 100.00% 23
5000 341 45 147 429 17.20 17.40 17.60 17.80 m/z~> aphoant 1 96 117 I 179 207225 251 281 311 L A 397 ’LHurmhmnam—ummmummnmmuuEummmPIETTTR m/z 341.00 40 60 80 100120140160180200220240260280300320340360380400420 ( 29.87% Abundance #48337:2H-1,4-Benzodlazepin-2-one, 7-chloro-1,3-dihydro-5- 73 341
.................... ............................ 1ndn/d/n//d10/m/n/d-noaononon, 5000 17.20 17.40 17,60 17.80 45 m/z 147.00 14.64% 91 I 116 146 , TpmmmmPmg 227 269 315 L I TtTTTyTTTTp-tTTp-TTTp-rTTTTlTTfiTrT^^ m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714: 1.1.1.5.7.7,7-Heptamethyl-3.3-bis(trimethylsiloxy)t 73 / ■ ■ । ■11 ■ ■ ■ ■ ।1 • • ■ । • 147 17.20 17.40 17.60 17.80 5000 267 m/z 325.00 9.84% 355 429 45 ; 207 nPnumOmnuBppnm—vmppagt Tnuadmpnun—nn—mnamm121 miz-> Abundance 40 60 80 100120140160180200220240260280300320340360380400420
73 #56734:3-Trimethylsilyloxystearic acid, trimethylsilyl est a 17.20 17.40 17.60 17.80 m/z 342.00 9.82% 5000 147 233
313 429 387...... mmmmmmmkmmpmmm TVPTi TICUBUTTEMIT 189 I 339 T PP T m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
30602.D GCMS0103.M Thu Jan 10 15:45:07 2002 Page 3
NYC-WTC_000017255
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NYC-WTC_000017255Source: NYC Law Department, mirrored locally
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1 shared topics · Same agency, volume and box · similarity 0.993
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Laboratory report of GCMS analysis for sample AD28860 conducted on December 16, 2001, showing compound identification.
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1 shared topics · Same agency, volume and box · similarity 0.992
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