NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 19 pages
GCMS analysis results, sample AD30602, January 2002
Machine-extracted title · confidence 85%Gas chromatography-mass spectrometry analysis report for sample AD30602 showing detection of 2,4-DDD and other unknown compounds, analyzed January 22, 2002.
NYC-WTC_000017246–000017264Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\30602.D Vial: 30 Acq On : 28 Dec 2001 6:18 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 3-Isopropoxy-1,1,1,7,7, 7-hexam Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 20.28 2.93 ug/1 1347750 Acenaphthene-dl0 20.56 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopr^oxy-l,1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 42 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 3 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 12 4 Phos; toric acid, 3-(ethoxyimino)-2- 429 C14H36NO6PSi3 055334-96-8 10 Abundance j Scan 1659 (20.279 min): 30602.D (-) m/z 73.0.0 100.00% 73
5000 147 281 327 45 221 zot 20.00 20.20 20.40 20.60 — I11n 117 Pi rfih a 191 Pi"251 .. 353.383 415 Tr.............................................. m/z 147.00 37.14% mlz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
... MT iiii 5000 147 20.00 20.20 20.40 20.60 221 281 m/z 281.00 3 6.01% 327____ 415 _____ 519 561 -TI ' ' i 1 ' m/z-> 50 100 150 200’250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1.1.5.5.5-hexamethyl-3,3-bis[(trimet 73 147 281 20.00 20.20 20.40 20.60 5000 m/z 326.90 14.70% 369 207 249, 338 I miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily 73 20.00 20.20 20.40 20.60 m/z 282.00 9.71% 327 5000 237 45
Trk, .......147 1172 212 । 1। ■ i z ' 1_________________________ r i • ■ ' ■ i ■ ■ ■ 1 i ■ ■ ■ ■ i ■ ■ ■ ' i ■ • miz-> 50 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60
30602.D GCMS0103.M Thu Jan 10 15:45:12 2002 Page 4
NYC-WTC_000017256
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1 shared topics · Same agency, volume and box · similarity 0.992
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