NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 23 pages
GCMS analysis results for sample AD30633, Jan 2002
Machine-extracted title · confidence 95%Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.
NYC-WTC_000017210–000017232Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\30633.D Vial: 27 Acq On : 28 Dec 2001 3:23 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 17.45 7.00 ug/ 2966410 Naphthalene-d8 15.28 Hit# of 5 ntative ID MW MolForm CAS# Qual 1 1,1,1,5,7. /,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 2 2H-1,4-B zodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 3 3-Trimet hylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 9 4 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 9 Abundance /...... Scan 1351 (17.450 mln): 30633.D (-) m/ Z 73.0,0 100.00% 73
5000 341 147 45 , 97 117. [ 179.207225 251 281 311 L I . 429 17.20 17.40 17.60 17.80 i । TTTTjTn-r]T TTgmmmgmanmanmpe0an—an——mma2000ugnpngnoe1’0110—00110311000117 397 L m/z 341.00 28.84% miz-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 147 5000 267 355 429 17.20 17.40 17.60 17.80 1 45 207 m/z 147.00 14.26%
m/z-> Bump*unu—u“uOp—umnmr M -p-nTpTrrprrr ini,. 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #48337: 2H-1 4-Benzodiazepin-2-one 7-chloro-1,3-dihydro-5- 73 341 1 • ■ • i ■ ■ • ■ / ' • • • i' ■ ■ • i • ■ ■ 17.20 17.40 17.60 17.80 5000 i " m/z 342.00 9.84% 45 91 i ; 116 146 227 269 mmp—pmpmngmmemmmmmOTTITp 315 Tr. । H « 11 < > > i । i > i < 111 i > j i m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #56734: 3-Trimethylsilyloxysteartc acid, trimethylsilyl est 73 17.20 17.40 17.60 17.80 m/z 325.00 9.65% 5000 147 233
313 429
m/z~> ............... ... 182,1..10.47..1.70070047330../..37.I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440 T 1441** 17.20 17.40 17.60 17.80
30633.D GCMS0103.M Thu Jan 10 15:23:47 2002 Page 4
NYC-WTC_000017220
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NYC-WTC_000017220Source: NYC Law Department, mirrored locally
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
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