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GCMS analysis results for sample AD30633, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.

NYC-WTC_000017210–000017232

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\30633.D Vial: 27 Acq On : 28 Dec 2001 3:23 pm Operator: 209 GALOS Sanpl e : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Propanone, 1-(1-methylethoxy Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T. 18.16 0.57 ug/1 256342 Acenaphthene-dl0 20.56 Hit# of 5 Tentative ID MW MolForm CAS# Qual l 2-PropanoneyI-(1-methylethoxy)- 116 C6H1202 042781-12-4 25 2 2 (5H)-Fur; none, 3,5,5-trimethyl- 126 C7H10O2 050598-50-0 23 3 4-Hepten- -one, (E)- 112 C7H120 036678-43-0 9 4 Butane / 58 C4H10 000106-97-8 9 Abundance Scan 1428 (18.157 min): 30633.D (-) m/z 43.00 100.00% 43 57 73 5000 111 95 —TRTTTTTTui v. । >■ । > > r» 17.80 18.00 18.20 18.40 m/z-> mlll. 11 nhIrhni । rh 11111 ′ 111 85 :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 12713g 146 > 4 l'l,।. ."I...... p । । 201 , m/z 57.00 70.41% Abundance* #3286: 2-Propanone, 1-(1-methylethoxy)- 43

5000 - TTTTPT 1-15 i MTPITTu III IT 17.80 18.00 18.20 18.40 27 m/z 73.00 58.83% I 11|. 58 Il 73l •I" ’ ‘ I ‘ .. j rr.. ।... i | ।।■ 11 ■ > 11 >>> 1111 > i. 1111111111 j 11 ■ 1111111111 ■ 111111 r. 1111 ■ 11111111 miz-> ;20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance> #4475; 2(5H)-Furanone, 3.5.5-trimethyl- 43 <i e । P 141 ppm । । Pig) 17.80 18.00 18.20 18.40 5000 111 m/z 111.10 46.98% 83 55 126 68 . .......................................... .................................................. ..................... m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #2569:4-Hepten-2-one, (E)- 43 17.80 18.00 18.20 18.40 * m/z 41.05 28.18% 5000

55 69 83 94 112 TTmumupmOmmm—*nme—up——pImTmPemWmmpT =P*RRT miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 17.80 18.00 18.20 18.40

30633.D GCMS0103.M Thu Jan 10 15:23:53 2002 Page 5

NYC-WTC_000017221

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NYC-WTC_000017221Source: NYC Law Department, mirrored locally

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