Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
NYC-WTC_000017171–000017191Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\lNSTRU~l\209\DATA\DEC2701\30607.D Vial: 33 Acq On : 28 Dec 2001 9:15 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
17.45 3.94 ug/1 1524070 Naphthalene-d8 15.28
Hit# of 5 Tent at ive/1D MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 38 2 l,l,l,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 3 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 9 4 Silane, [1,2, ^benzenetriyltris (oxy 342 C15H30O3Si3 017864-23-2 9 Abundance Scan 1351 (17.449 min): 30607.D (-) m/z 73.0,0 100.00% 73
5000 341 ______ /________ 147 1*1***I*’1’I-**I*’ 45 _ 429 17.20 17.40 17.60 17.80 96 117 [ 179,207225 251 281 311 L _ 397 . OWn Tmdmpmnm3m1pn1m0 —u—uuun“TCCTT1’T !,,,. ।....!. <., |, n. । > m/z 341.00 28.89% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 5000 17.20 17.40 17.60 17.80 147 m/z .147.op 14.06% 117 [ 207 267 311 TnnungnmmmnmmRa—nmmmmupn m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714:1.1.1,5,7,7.7-Heptamethyl-3.3-bis(trimethylsiloxy)t 73
147 17.20 17.40 17.60 17.80 5000 267 rn/z 342.00 9.64% 355 429 45 207 Ml, 1.... 1I... 11.... 1.... 1.1 I1.... 1.1I... 111 n | It ___________________ a___ ।...»j.... j... । j i». 111». H . miz-> 40 60 80 100120140160180200220240260280300320340360380400420 — [ I I I . ) y I J — I I I I Abundance #48337:2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 73 341 17.20 17.40 17.60 17.80 m/z 325.op 9.17% 5000 45 91 1 I 116 146 227 269 315 [ 1 M T T ।. ,1111. .11.. 11 p'l.. ].... ।.... 1.1..!.... 1..'..,..,. 1111111 Ji i fl 1111,1111111 r p 111111,11 r T I ’ ‘ ' • | » ‘ ‘ ‘ I • ' m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17,60 17.80
30607.D GCMS0103.M Thu Jan 10 14:55:48 2002 Page 4
NYC-WTC_000017181
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NYC-WTC_000017246
Gas chromatography-mass spectrometry analysis report for sample AD30602 showing detection of 2,4-DDD and other unknown compounds, analyzed January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017210
Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018882
GCMS analysis report for sample AD30488 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017299
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30634 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017192
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018898
GCMS analysis report for sample AD26827 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017630
Laboratory report documenting GCMS analysis of sample AD31023 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017595
Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017144
Laboratory report documenting GCMS analysis of sample AD30601 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000017118
Fragmented administrative record from the DEP laboratory files dated January 2002 regarding environmental sample processing.
Filed in the same folder
NYC-WTC_000017119
Laboratory record showing method validation parameters including drip rates and pH for DEP samples in January 2002.
Filed in the same folder
NYC-WTC_000017122
Laboratory calibration report from the DEP testing for volatile organic compounds using GCMS analysis on December 28, 2001.
Filed in the same folder
NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
Filed in the same folder
NYC-WTC_000017139
Laboratory report listing quantitative results for numerous organic compounds in sample AD30601 analyzed on January 10, 2002.
Filed in the same folder