Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
NYC-WTC_000017126–000017138Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\INSTRU~1\209\DATA\DEC2701\LBB.D Vial: 24 Acq On : 28 Dec 2001 12:26 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclohexasiloxane, dodecamethy Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
17.45 1.41 ug/1 654866 Naphthalene-d8 15.29
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl- 444 C12H36O6Si6 000540-97-6 38 2 l,l,l,5,7,2<7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 16 3 Silane, J1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12 4 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 9 Abundance Scan 1352 (17.452 min): LBB.D (-) m/ z 73.0,0 100.00% 73
5000 341 ‘"41 1 ‘ 1............ .-Tl f l ( i . । < i 147 429 17.20 17.40 17.60 17.80 45 117 . [ 179.297225 251269 295 323 t 397 1 I , L^nh^r -p-rrtp-TEnunuuDum—uEum“IOD8AT | H | ‘ ‘ I ‘ ‘ I ‘ m/z 341.00 30.36% mz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 5000 । ■ । ■ । i । r1 ■ i ■■ । । । r > । 17.20 17.40 17.60 17.80 147 m/z 147.00 13.80% 117—"nTuemmpn I 207 267 311 [ Tuun—m——m—m)—nm mkmmmmmmmmp m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714: 1.1.1.5.7.7.7-Heptametnyl-3,3-bis(trimethylsiloxy)t 73 21 ’ • • • i ’ • • • i • * ‘ ‘ i • • ' * i 4 ’ »
147 17,20 17.40 17,60 17.80 5000 267 m/z 342.00 10.66% 355 429 45 207
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance 73 #73587: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- 239 T L. 17.20 17.40 17.60 17.80 18" i m/z 325.00 10.09% 342 5000
45 133 211 Tp Thu—u—a—poooT .. 1111. ।. ni p. ।. j ii 11 |T> > 11 h > 1111111111 > 1111 11 __________ m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17,60 17,80
LBB.D GCMS0103.M Thu Jan 10 13:58:41 2002 Page 3
NYC-WTC_000017134
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NYC-WTC_000018882
GCMS analysis report for sample AD30488 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017144
Laboratory report documenting GCMS analysis of sample AD30601 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017542
Laboratory report documenting GCMS blank analysis for volatile organic compounds on sample AD30605 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018898
GCMS analysis report for sample AD26827 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018817
Laboratory report of GCMS analysis for sample AD28860 conducted on December 16, 2001, showing compound identification.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017246
Gas chromatography-mass spectrometry analysis report for sample AD30602 showing detection of 2,4-DDD and other unknown compounds, analyzed January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017192
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017299
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30634 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000017118
Fragmented administrative record from the DEP laboratory files dated January 2002 regarding environmental sample processing.
Filed in the same folder
NYC-WTC_000017119
Laboratory record showing method validation parameters including drip rates and pH for DEP samples in January 2002.
Filed in the same folder
NYC-WTC_000017122
Laboratory calibration report from the DEP testing for volatile organic compounds using GCMS analysis on December 28, 2001.
Filed in the same folder
NYC-WTC_000017139
Laboratory report listing quantitative results for numerous organic compounds in sample AD30601 analyzed on January 10, 2002.
Filed in the same folder
NYC-WTC_000017144
Laboratory report documenting GCMS analysis of sample AD30601 including DDD surrogates on January 22, 2002.
Filed in the same folder