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GCMS analysis results for sample AD30601, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.

NYC-WTC_000017126–000017138

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\LBB.D Vial: 24 Acq On : 28 Dec 2001 12:26 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 20.28 0.96 ug/1 475005 Acenaphthene-dl0 20.56 Hit# Of 5 ntative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 36 2 3-Isopropoxy-l, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 32 3 Propanedioic acid, [(trimethylsilyl 336 C12H2805Si3 038165-93-4 32 4 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 32 Abundance Scan 1660 (20.280 min): LBB.D (-) m/z 73.00 100.00% I 73

5000 147 281 327 m P ।। — 45 117 • ■ i • -+ TTT 191, 221 251 A 383 415 . 20.00 20.20 20.40 20.60 m/z 147.00 38.73% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147

5000 281 ’ ' I * —m 20.00 20.20 20.40 20.60 369 m/z 281.00 37.09% 207 249, 1111 ,338 I miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503; 3-Isopropoxy-1.1,1.7,7.7-hexamethyl-3,5,5-tris(trim 73 1 ‘ 1 i 1 * * * I r . , i' । ,1 < , < । i r ' f 20.00 20.20 20.40 20.60 5000 147 m/z 326.90 15.72% 221 281 . 327 415 519 561 — ' I " t J । » » J i j n i r ।" i 1 t i ] t r miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73507: Propanedioic acid, [(trimethylsilyl)oxy]-, bis(trim 73 20.00 20.20 20.40 20.60 m/z 282.00 10.72% 5000 147 45 102 1 1 i 1 ' ■ ■ i ■ Tfr 221 Mp4?,-TI ,. 222 321 ................... -IP -*P miz-> 50 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60

LBB.D GCMS0103.M Thu Jan 10 13:58:47 2002 Page 4

NYC-WTC_000017135

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NYC-WTC_000017135Source: NYC Law Department, mirrored locally

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