NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\INSTRU~1\209\DATA\DEC2701\LBB.D Vial: 24
Acq On : 28 Dec 2001 12:26 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/17 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 4 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
20.28 0.96 ug/1 475005 Acenaphthene-dl0 20.56
Hit# Of 5 ntative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 36
2 3-Isopropoxy-l, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 32
3 Propanedioic acid, [(trimethylsilyl 336 C12H2805Si3 038165-93-4 32
4 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 32
Abundance Scan 1660 (20.280 min): LBB.D (-) m/z 73.00 100.00%
I 73
5000 147 281
327 m P ।।
—
45 117
• ■ i • -+ TTT
191, 221 251 A 383 415 . 20.00 20.20 20.40 20.60
m/z 147.00 38.73%
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73 147
5000
281
’ ' I * —m
20.00 20.20 20.40 20.60
369 m/z 281.00 37.09%
207 249,
1111 ,338 I
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503; 3-Isopropoxy-1.1,1.7,7.7-hexamethyl-3,5,5-tris(trim
73
1 ‘ 1 i 1 * * * I r . , i' । ,1 < , < । i r ' f
20.00 20.20 20.40 20.60
5000
147
m/z 326.90 15.72%
221 281 . 327 415 519 561
— ' I " t J । » » J i j n i r ।" i 1 t i ] t r
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #73507: Propanedioic acid, [(trimethylsilyl)oxy]-, bis(trim
73 20.00 20.20 20.40 20.60
m/z 282.00 10.72%
5000
147
45 102
1 1 i 1 ' ■ ■ i ■ Tfr
221
Mp4?,-TI ,. 222 321 ................... -IP -*P
miz-> 50 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60
LBB.D GCMS0103.M Thu Jan 10 13:58:47 2002 Page 4
NYC-WTC_000017135
OCR can misread numbers and units. Confirm readings against the page image before using them.