NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC2701\LBD.D Vial: 38
Acq On : 29 Dec 2001 7:39 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/18 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 4 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
20.27 1.66 ug/1 835535 Acenaphthene-dl0 20.57
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 3 84 C12H3604Si5 003555-47-3 40
2 3-Isopropoxy-lyl, 1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38
3 Octadecanoic acid, 2-[(trimethylsil 386 C22H46O3Si 056196-58-8 10
4 Pho sphoric acid, 2-(methoxyimino) -3 415 C13H34NO6PSi3 _ 055319-85-2 9
Abundance Scan 1659 (20.272 min): LBD.D (-) m/z 73.0,0 100.00%
73
5000
147 281
45
327 20.00 20.20 20.40 20.60
- 117. 191 221 251
T—OB—T A 383 415. .. .... m/z 147.00 34.05%
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73 147
281
5000
20.00 20.20 20.40 20.60
369 m/ z 281.00 31.20%
207 249, 338 J..................
—
m/z-> 50 100 150 200 250 300 350 400 450 500 550
JAbundance #60503: 3 Isopropoxy-1.1.1,/ . ./-nexamethyl-3,5,5-tsttrim
73 ........ ..............
20.00 20.20 20.40 20.60
5000 m/z 326.90 11.80%
147
221 281 327 415 519 561
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #74126: Octadecanoic acid, 2-[(trimethylsilyl)oxy]-, methyl
73 20.00 20.20 20.40 20.60
327 m/z 74.00 8.74%
5000
371
103129 159
|
■ ■ i ■ 1
mz-> 50 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60
LBD.D GCMS1126.M Mon Jan 28 11:39:14 2002 Page 4
NYC-WTC_000004200
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