Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\LBD.D Vial: 38 Acq On : 29 Dec 2001 7:39 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclohexasiloxane, dodecamethy Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
17.45 2.05 ug/1 953897 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 23 2 1,1,1,5,7,7,7-Heptaimethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 23 3 2H-1,4-Benzodiazepi n-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 4 Silane, [1,2,3-be: enetriyltris(oxy 342 C15H30O3Si3 017864-23-2 16 Abundance Scan 1352 (17.454 min): LBD.D (-) m/z 73.00 100.00% 73
5000- 341 ...................... ............................... 147 429 17.20 17.40 17.60 17.80 45 i 117 ( 179 207225 251 281 311 L i 11010—0101—0011000117712" TTT< > p 11 > 11 <. > 1 rn. | > 397... L m/z 341.00 31.64% m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 -— 5000 17.20 17.40 17.60 17.80 147 m/z 147.00 13.85% I 117 |. 207 267 311 [ I " ■' i" " i ■ ■" i" " i" " i ■"1 r1 ■ ■ r ■ ■ ■ r "11 ■'' ■ i" " I" " r "' i" " i"1' i" " i '' ■ i'1'11' ■'' i1 ■ m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance “56714: 1.1.1.5,7.7,7-Heptamethyl-3.3-bis(trimethylsiloxy)t 73 .......... .................................... 147 17.20 17.40 17.60 17.80 I 267 m/z 325.00 10.91% 5000 ft I 355 429 I 207 45 i r ",,■ ,i ,■ ,‘..... ,,, ....... "1 ■ i.................................. ‘"11" r r1" r "' r "1 r ...... r H....... i " i" "i t"■r"■i r'" i"" i" " i" " i"1 ■ i ■ m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 ..... A......... Abundance #48337: 2H-1 ,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 73 341 17.20 17.40 17.60 17.80 m/z 342.00 10.48% 5000- 45 91 TTTTjrrrTpT 116 WI—I——B———u———146 —u—269 ......... 227... —0201m0m01u00 .....315 0EOONTT 1" i" " i'1" i" " i1"' r m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 17.20 17.40 17.60 17.80
LBD.D GCMS1126.M Mon Jan 28 11:39:09 2002 Page 3
NYC-WTC_000004199
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
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