NYC-WTC_000035776
Laboratory data sheet recording GCMS analysis of a blank sample for nitrosamines and chlorinated compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Document / 13 pages
GCMS calibration results for sample AD28662, Dec 2001
Machine-extracted title · confidence 100%Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.
NYC-WTC_000034958–000034970Folder label: “GCMS X 11/24/01 A 12/4/01”
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NYC 9/11 Public Portal Document Library Search Compound Report ‘ Data File C:\HPCHEM\1\DATA\DECO4O1\LB. D . Vial: 3 Acq On 4 Dec 2001 2:19 pm Operator: 209 GALOS Sample lb 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclohexasiloxane, dodecamethy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 17.48 1.72 ug/1 545796 Naphthalene-d8 15.32 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cy clohexasiloxane ,dodecame thyl- 444 C12H3606Si6 000540-97-6 34 2 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 14 3 Silane, [1,2,3-benzenetriyltris (oxy 342 C15H30O3Si3 017864-23-2 11 4 3-Trimethylsi loxystearic acid, tr 444 C24H5203Si2 000000-00-0 9 Abundance 73 Scan 1354 (17.476 min): LB.D (-) m/z 73.00 100.00%
5000- 341
147 429 ‘r 1.' 1 T ' i ' 1 T-r-p-T
45 17.20 17.40 17.60 17.80 | TTTETTEUIETETTI" 1 117 179,. 207225 251 281 311 L ; 397 TI—g"nggTT[ ’THTTNgTITTTTTTTTTTTT , m/z 341.00 38.89% tnfz-> 40 60 80 100120140160180200220240260280300320340 360380400420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341 % 429 T-r-p-r 5000 17.20 17.40 17.60 17.80 147 m/Z 147.00 17.44% I............. ( 117...... |............. 207 267 311 [ . TTTTTTTTT TTTTTCIT . 11111 ■ 111 r, r i . j ... H... 11.11111111111 mm m/z-> 40 60 80 100120140160180 200220240 260280300320340 360380400420 Abundance #48337: 2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 73 341 T ‘ | • ■ ■ • । ----- 17.20 17.40 17.60 17.80 5000J m/z 342.00 12.99% 45 91 I 116 146 227 269 315. nTTT TTTTTTTTT TTTTTTTTT TTTTTTTTTT"T’T’TETTTTTTTTTTT miz-> 40 60 80 100120140160180200220240 260280300320340 360380400420 ............... ----- Abundance #48324: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- I ' ' I 1 73 17.20 17.40 17.60 17.80 m/z 429.05 12.29% 239 5000 342
m/z—> 45 133 179 211 I —"T’IUTTE ’I1100000111—9T"TT9-I’E— —ETITEI"TTT • • •'l■•••l> • 40 60 80 100120140160180200220240260280300320340360380400420 —3’44— l■■ •■l ■ ■•■l ■ ■■ ■ I■ .. 4.. 17.20 1 7.40 17.60 1 7.80
LB.D GCMS1126.M Thu Dec 06 14:40:54 2001 Page 2
NYC-WTC_000034965
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NYC-WTC_000034965Source: NYC Law Department, mirrored locally
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