Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 7 01\LBD.D Vial: 38 Acq On : 29 Dec 2001 7:39 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
14.31 0.56 ug/1 259236 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasil ane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Benzoic acid/ 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 47 3 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 46 4 N- (Trifluoroacetyl)-O,O',O' '-tris(t 481 Cl9H3 4 F3N04 S i 3 000000-00-0 37 Abundance Scan 1009 (14.305 min): LBD.D (-) m/z 72. 95 100.00% 73
5000 267 355 45 , 14.00 14.20 14.40 14.60 108125 154 177 193 . 223 251 323339 i, " I" " I' " ‘ I 111 —n—ummmmummm *— m/z 267.00 34.14% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyciopentasiloxane, decamethyl- 73
355 267 5000- 14.00 14.20 14.40 14.60 ' ' ' m/z 355.05 23.30% 191207 251 i 323339 110B‘0—1TT1—B211100111121110111—C910UB3I0—ITITT ” ■ ■ i ■ ■ ■' i " 1 ■ I' ■'' 'i ■ ■ i" " l m/z->40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73978: Benzoic acid. 2.5-bis(trimethyisiloxy)- trimethyls 73 355 1-1 "I 1 1 1 1 I 14.00 14.20 14.40 14.60 5000 m/z 74.00 8.91 45 | I 147 179 207223 267282 m/z-> " ■ i'' 40 i ■ ■" । ।‘ ■ i ■ ‘" i"1 ■ ।। 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ■ i1" ■ ।■ i" " i1 ■ ‘' ।■ i ■" ■ i ■ ■" i ■"11
Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsiiyl)- 73 14.00 14.20 14.40 14.60 m/z 356.05 8.77% 5000 267 17$ 356 45 147 TT| A I I ‘| I I > | I I I I | I I I I | I I I I | IV, I | i , I ,} 209 237 , | 312 l____ TTT '' i " ■ i ■' ■11'1 " r ■ " i''' ■ i'' i ■ ■ • ■ । i 1 ' ■ ■ i ' ' ■ ’ i miz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60
LBD.D GCMS1126.M Mon Jan 28 11:39:05 2002 Page 2
NYC-WTC_000004198
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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