Laboratory report documenting GCMS blank analysis for volatile organic compounds on sample AD30605 conducted on January 10, 2002.
NYC-WTC_000017542–000017555Folder label: “GCMS X 12/20/01 A 1/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\LBB.D Vial: 18 Acq On : 9 Jan 2002 5:55 am Operator: 209 GALOS Sample * : gems scan 12/20a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.
20.13 0.88 ug/1 274856 Acenaphthene-dl0 20.39
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, A., 1,1,5,5, 5-hexamethyl 384 C12H3604Si5 003555-47-3 53 2 3-Isopropox/-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 10 3 Octadecanoic acid, 2-[(trimethylsil 386 C22H46O3Si 056196-58-8 10 4 4-Amino-5-/imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 9 Abundance Scan 1643 (20.125 min): LBB.D (-) m/ z 73.0,0 100.00% 73
5000 147 281 45 191 . 221 251 [ 327 K 383.415 19.80 20.00 20.20 20.40 — . 117^ . , . *1——*** m/z 147.00 34.35% miz-> 50 166 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 281 5000 1PII 19.80 20.00 20.20 20.40 369 m/z 281.00 31.35% 207 249, 338 [ —I ---PI‘1**1444111144141141*114*1 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503; 3-Isopropoxy-1.1,1.7,7,7-hexamethyl-3,5,5-tris(trim 73 19.80 20.00 20.20 20.40 5000 m/z 326.90 11.90% 147 221 281 327 415 519 561 m/z-> sb' ‘ 100 150 ‘ 266 250 ' ' 300 350 ' ' 400 ' ‘ 450 500 ' ‘ 550 Abundance #52732: Octadecanoic acid, 2-[(trimethylsilyl)oxy]-, methyl ‘ * I ' ' * ‘ l TI T T 73 19.80 20.00 20.20 20.40 m/z 282.00 9.55% 5000 327 103 371 | | 149 159 - —— ‘ ‘ I ‘ ‘ 1 ' I * ’ I • ' ' ' I • ' ‘ * I m/z—> 50 100 150 200 250 300 350 400 450 500 550 19.80 20.00 20.20 20.40
LBB.D GCMS0103.M Thu Jan 10 16:15:25 2002 Page 5
NYC-WTC_000017552
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NYC-WTC_000017571
Laboratory report documenting GCMS analysis of sample AD30903 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017630
Laboratory report documenting GCMS analysis of sample AD31023 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017556
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31019 performed on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017595
Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017615
Laboratory record of GCMS analysis identifying other unknown compounds in sample AD30902 on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018650
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30906 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018882
GCMS analysis report for sample AD30488 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000017529
Document page containing no readable text or identifiable content for description purposes.
Filed in the same folder
NYC-WTC_000017530
Unreadable document containing GCMS analytical data from the Department of Environmental Protection dated January 2002.
Filed in the same folder
NYC-WTC_000017533
Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.
Filed in the same folder
NYC-WTC_000017537
Laboratory report listing quantitative results for numerous organic compounds in a GCMS reference scan of sample AD30605 on January 9, 2002.
Filed in the same folder
NYC-WTC_000017556
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31019 performed on January 18, 2002.
Filed in the same folder