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GCMS analysis log for sample AD31019

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31019 performed on January 18, 2002.

NYC-WTC_000017556–000017570

Folder label: “GCMS X 12/20/01 A 1/9/02”

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NYC 9/11 Public Portal Document Library Search Compound Report . Data File : M:\INSTRU~1\209\DATA\JAN0802\31019.D Vial: 24 Acq On : 9 Jan 2002 12:45 pm Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE. Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peeeeerrrrrrrrrrsr Serres rr: Srerrerre rrr rrrr rrr errr errr rere rer rss r eT Peak Number 4 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 3 R.T. | EstConc Area Relative to ISTD R.T. 20.13 1.69 ug/l 645088 | Acenaphthene-d10 20.39 Hit# of 5 Tenjétive ID MW MolForm cas# Qual 1 Trisiloxane,/1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 2 3-Isopropo#y-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 36 3 4-Amino7Z-imidazole carboxamide, tr 342 C13H30N40Si3 000000-00-0 22 4 Octadeg4noic acid, 2-[(trimethylsil 386 C22H4603Si 056196-58-8 22 Rbundance ‘Scan 1643 (20.127 min): 31018.D ¢) m/z 73.00 100.00 : ow 147 281 opr | 48 21 sr 415 '19.80_20.00 20°20. 20.40, | Mh MES, fe w/z 147.00 35.06! mi>__80 100 150.200 _250 300 _380_400__450_500_850 ‘Abundance WERASD Tetons, 1.1.75. 8 Rexam SB eet | . Hi 5000 | f 19.80_20.00 20.20 20.40 i 369 m/z 281.00 32.55 \ 207 249, 338 z—> a 150 __200 250 300 350 400 450 500 550 undance | 7s #60803: Sisopropoxy-1,1.1,7.7,7 hexamethyr-3,5.5-tris(inim | 19.80 20.00 20.20 20.40 | 8000: m/z 326.90 12.86 | wr (| | i | 221 281 a7 as a mz> 50. 100 _150__200 250 300 350 400 450 500 550_ Abundance = #48317: 4-Amino-B-imidazole carboxamide, tris(timethyisily ~~ T 1 19.80 20.00 20.20 20.40 | m/z 282.00 9.06' 37 i c 1 5000: i 237 | i 45 | Ware 212 | maz>__80 _100 160 __200 250300 _350___400__450__500__550_| 19.80 20.00 20.20 2040 31019.D GCMS0103.M Thu Jan 10 16:01:31 2002 Page 4 NYC-WTC_000017565

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GCMS calibration results · Box DEP Box 16

NYC-WTC_000017533

Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.

Filed in the same folder

GCMS reference scan results · Box DEP Box 16

NYC-WTC_000017537

Laboratory report listing quantitative results for numerous organic compounds in a GCMS reference scan of sample AD30605 on January 9, 2002.

Filed in the same folder

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