Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.
NYC-WTC_000017192–000017209Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01”
OCR status: ocr · source: ours
NYC 9/11 Public Portal Document : Library Search Compound Report 7 Data File : M:\INSTRU~1\209\DATA\DEC2701\30608.D Vial: 32 Acq On : 28 Dec 2001 8:16 pm Operator: 209 GALOS Sample + GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ee eeererrrrrre erro re terre rrrrrrrrtrr rrr rit tittrrtrrrr irri itt r tras Peak Number 5 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 3 R.T. EstCone Area Relative to ISTD R.T. 20.28 1.96 ug/1 839991 Acenaphthene-d10 20.56 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,%;5-hexamethyl 384 C12H3604Si5 003555-47-3 42 2 3-Isopropoxy-1,1,1,777,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 3 4-Amino-5-imidazoJ€ carboxamide, tr 342 C13H30N40Si3 000000-00-0 10 4 Octadecanoic acid, 2-[(trimethylsil 386 C22H4603Si 056196-58-8 9 indance "1650 (20.278 min}: 80608. (-) m/z 73.00 100.00 | | | 5000 ur 281 | 45 497, 191 224 251 T asp 289 48 20,00 20.20 _2040 20.60 | L sp ~rrrprr| m/z 147.00 35.94% > 50. 100 __150 200 250 300 350 _ _400 _450 550. Abundance #52459; Tislloxane, 1,1,1,5.5,shexamethy-3,9| timer i " | 281 | [Pamameee | | 20.00 20.20 20.40 20.60 | | 30 m/z 281.00 34.90% | 207 49, 338 | bvz—> 50 400 __150 200 250 300 350 400 450 500 550 ‘Abundance FG0ECS: STeopropory-1,1.1,7./ 7 hexamethyrs 5 Barstini 73 | 20.00 _20.20 20.40 20.60 5000 m/z 326.90 14.26% 147 a 281 sar 415 519581 : > 50. 400 __150__200 __250__300 _350 400 450 500 _ 550 Abundance 8317: -Amino-Smidazole carboxamide, tis(rimethyislly 0 20.00 _20.20 20.40 20.60 | m/z 282.00 9.618 | 307 I 5000: | 237 | Ware 212 7 imi 50 100 150-200-250 300350. 450. 10 550. 20.00 20.20 20.40 20.60 30608.D GCMS0103.M Thu Jan 10 15:08:11 2002 Page 5 NYC-WTC_000017203
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NYC-WTC_000017299
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30634 performed on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017157
Instrument output from a gas chromatography-mass spectrometry scan of sample AD30604 conducted on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017233
Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD30603 on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017144
Laboratory report documenting GCMS analysis of sample AD30601 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018882
GCMS analysis report for sample AD30488 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017246
Gas chromatography-mass spectrometry analysis report for sample AD30602 showing detection of 2,4-DDD and other unknown compounds, analyzed January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018817
Laboratory report of GCMS analysis for sample AD28860 conducted on December 16, 2001, showing compound identification.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017595
Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017556
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31019 performed on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017615
Laboratory record of GCMS analysis identifying other unknown compounds in sample AD30902 on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018898
GCMS analysis report for sample AD26827 showing detection of unknown compounds and surrogate recovery data from December 21, 2001.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000017118
Fragmented administrative record from the DEP laboratory files dated January 2002 regarding environmental sample processing.
Filed in the same folder
NYC-WTC_000017119
Laboratory record showing method validation parameters including drip rates and pH for DEP samples in January 2002.
Filed in the same folder
NYC-WTC_000017122
Laboratory calibration report from the DEP testing for volatile organic compounds using GCMS analysis on December 28, 2001.
Filed in the same folder
NYC-WTC_000017126
Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.
Filed in the same folder
NYC-WTC_000017139
Laboratory report listing quantitative results for numerous organic compounds in sample AD30601 analyzed on January 10, 2002.
Filed in the same folder