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GCMS analysis log for sample AD30608

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.

NYC-WTC_000017192–000017209

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017204
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NYC 9/11 Public Portal Document 5 Library Search Compound Report e Data File : M:\INSTRU~1\209\DATA\DEC2701\30608.D Vial: 32 Acq On : 28 Dec 2001 8:16 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L. eeteetrerrrrr referrer ererrrrrrrrrrrtrrrrrtirrrtrtitt ttt rrr rrr rrr ty Peak Number 6 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 6 R.T. | EstConc Area Relative to ISTD R.T. 21.07 0.54 ug/1 233516 | Acenaphthene-d10 20.56 Hit# of 5 Tentative ID MW MolForm cas# Qual Benzoic acid,A-ethoxy-, ethyl este 194 C11H1403 023676-09-7 94 2 Ethylparabe; 166 C9H1003 000120-47-8 53 3 Methylparg¥en 152 C8H803 000099-76-3 43 _4 Anisyl ionate 194 C11H1403 007549-33-9 43 bundance Cl aa | m/z 120.95 100.008 | s000 149 i 65 138 ad ! 39 59, 78 05 108 106 ‘20.80 21,00 24:20. 24.40 i m/z 149.0) 48.53% mmiz->__20 30 40 50 60 70 80_90 100 110 120 130 140 150 160 170 180 190 200 ‘Abundance He12b0: Bene ace, ctor ey ester i 5000 = 198 104 20:80. 21:00 21.20 21.40 | - a 03 i Nes m/z 194.0, 27.80% | I hve __20 30_40 50 60 70 89) 90 100 110 120 130 140 150 160 170 180 190 200 ‘Abundance sek Enybarer | —""20'80 21100 21202140 +5000 m/z 138.0, 25.56% 65 93 138 166 . kd ime> 20 30 40. 80 60 70 80 90 100 110 120 130 140 180 160 170 100 190 200. ‘Abundance i— #66000: Methylparaben i Ht 20.80 21.00 21.20 71.40 | m/z 65.0, 21.86% | S000 152 on 93 48 miz-> 20 3040 50 60 70 60 90 100 110 120 130 140 150 160 170 180 190 200, 20.80 21:00 21129 21.40 30608.D GCMS0103.M Thu Jan 10 15:08:16 2002 Page 6 NYC-WTC_000017204

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NYC-WTC_000017204Source: NYC Law Department, mirrored locally

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