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GCMS analysis log for sample AD30608

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.

NYC-WTC_000017192–000017209

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017205
OCR text

OCR status: ocr · source: ours

NYC 9/11 Public Portal Document Library Search Compound Report . Data File : M:\INSTRU~1\209\DATA\DEC2701\30608.D Vial: 32 Acq on + 28 Dec 2001 8:16 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst. : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ISSO ISIS EISSN IEI ISIE IS IIE SIE IAI OIG IOII OIC IO IOI II TIT IA TI Peak Number 7 Benzeneethanamine, N-[(pentafl Concentration Rank 5 R.T. EstCone Area Relative to ISTD R.T. 22.79 1.18 ug/1 499871 Phenanthrene-d10 24.99 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Benzeneethangfmine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 25 2 N-(Trifluoyéacetyl) -N,0,0',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 22 3 N-(Triflygracetyl) -0,0',O"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 22 4 N-(TrifYforoacetyl) -0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 22 uundance, ‘Scan 1933 (22.783 min}: 30608. ¢) m/z 73.00 100.00 | | | t 5000- | } 147 355, | 45 ana 401 | "zalao”22'60"22'e0 "za'00 25°20 3ar x Meh ete be PS m/z 355.05 29.008 niz-—> _§0 100 _ 150 __200__250 __300 __350__400___450__500_550. indanics #74706: Ber@eneeihanamine, N-|(pentafluoropheny)methyiene} | 355 | | 5000 | sy | 22.40 22.60 22.80 23.00 23.20 é m/z 147.00 28.37 pret 261 386 458 548. epreeryere ey SB pe Ee Wz-> "80100 180. 200 250 300. 350 400450 600 580 indance a (#60162; N-(Thiflucroacetyl)-N.O.0°O"tetrakis(trimethyisi | | | 355 -| 22.40 22.60 22.80 23.00 23.20 | 000 m/z 221.0, 20.324 | aa 147_ 193 267 538 mlz > 50 100 150200 250 350 400 450 500550 indance: "#58807: N-(Trifluoracetyi)-O,0",O"-tris(timethyisiiy)jepin 22.40 22.60 22.80 23.00 23.20 365 m/z 281.00 16.81% 1 | s000} | bi 140 184 281 480, L. 50100150200 250 300350400450 500850 | 2240 22160 22180 23.00 23.20 30608.D GCMS0103.M Thu Jan 10 15:08:22 2002 Page 7 NYC-WTC_000017205

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NYC-WTC_000017205Source: NYC Law Department, mirrored locally

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