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GCMS analysis report for sample AD31022, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.

NYC-WTC_000017595–000017614

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017608
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NYC 9/11 Public Portal Document . : Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31022.D Vial: 21 Acq On : 9 Jan 2002 9:49 am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library + C:\DATABASE\NBS75K.L. Te IGN EIEIO III TOSI III III II IIIS IT TOIT IIT I III III IIIS Peak Number 7 Benzeneethanamine, N-[(pentafl Concentration Rank 6 R.T. | EstCone Area Relative to ISTD R.T. 22.64 1.90 ug/l 631020 Phenanthrene-d10 24.81 Hit# of 5 éntative ID MW MolForm cas# Qual 1 Benzeneefhanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 2 N. (trig@uoracetyl) -0,0',O"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 3 N- (Tr¥Fluoroacetyl) -0,0',O''-tris(t 481 C19H34F3N04S13 000000-00-0 37 4 N-(peifluoroacetyl) -N,0,0',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 35 (Abundance ‘Scan 1947 (22.640 min): 31022.D (-) m/z 73.00 100. 00% i | | | S000 147 21 355 45 Gu 491 "22:40 22.60 22.80 23.00 3ar se x io eee bres aeepre| m/z 147.00 24.92 i> 50100 150200250 __300_350__400__450__500_550_ ‘Abundance #74706: Benzenesthanamine, N-[(pentafluorophenyimethylene) 355 7 i | 6000: i ‘22:40 22.60 22.80 23.00 i m/z 355.0, 24.42) | 1 208 251, 281 386, 458. 548 386 A tne ‘50 100. 150.200 250 300 350 _400_450_500_550 Readers CERRO NTivucrecolyF 0. OO trstramenyETy pI | 73 | bd 22.40 22.60 22.80 23.00 | 5000: m/z 221.05 18.39 | oe 140184 281 Hl 480 | 40 1 eee ee i> "30100150200 250 _ 300__350__400_ 490 _500_550 (Abundance #58326: N-(Trifiuoroacstyl)-O,0",O"-tis(trimethyisity))no AAA ABS Hl 2240 22.60 22.80 23.00 | 355 m/z 281.00 13.96% i 5000: 7 i | 45 i} 120147 193. 265 481 miz-> 50 400 150 200 250 300 350 _ 400 450 500 __ 550 22.40 22.60 22.80 23.00 31022.D GCMS0103.M Thu Jan 10 16:07:27 2002 Page 7 NYC-WTC_000017608

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NYC-WTC_000017608Source: NYC Law Department, mirrored locally

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Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.

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