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GCMS analysis report for sample AD30902, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis identifying other unknown compounds in sample AD30902 on January 18, 2002.

NYC-WTC_000017615–000017629

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017628
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NYC 9/11 Public Portal Document . Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\30902.D Vial: 20 Acq On : 9 dan 2002 7:51 am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L. TESA E SSH IIS ISIS ISI IO SII TIIO IGS IOI A TRIG I CII II TOIT IATA AIA Peak Number 7 Benzoic acid, 2,5-bis(trimethy Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.64 1.09 ug/1 359623 Phenanthrene-d10 24.80 Hit# of 5 Tentative ID MW = MolForm cAS# Qual 1 Benzoicfacid, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 43 2 N-(Trjfluoracetyl) -0,0',O"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 3 Bengéneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 4 N-ffrifluoroacetyl)-0,0',0!''-tris(t 481 C19H34F3NO4Si3_000000-00-0 43 Rbundanée "Scan 1916 (22.686 min): 30902.D () m/z 73.00 100.00: | S000 { | v mF a 7 401 '22140_22.60 22.80 23.00 ' St ob hrertererreeees| m/z 147.00 25.64 nz ‘50100150200 250 300 _350_ 400 _450_500__ 560 Abundance —~=~S*MY R978: Benzolc Seid, 2S-bis(timethyisliony)., timethys | ] 355, i. | 5000 ts 22.40 22.60 22.80 23.00 | 45 m/z 355.0, 22.86) i 447 479 223, 267 | 479 ad 297 i imiz> ‘50100150200 250 300-350 _400__480_500_560_| | Abundance FaweGF.A-CTiivo aoeky).O. OO trsitaimethyilly}epin | i id | Hl bia 22.40 22.60 22.80 23.00 000: m/z 221.05 17.41 via 140184 281 i 480 i | ene a eeeeaneal iniz> 's0 100180 200 250 300 350 _400_450__500_ 550 [Abundance #74706: Berzeneethanamine, N-(pentafuorophenyiymethyiene) | | 355 | *"’2alao "22160 '22!80 23.00 [m7z 281.00 13.19 | 5000 | . | i a 208 _251 261 388458 548. Inz-> __""'s0 100 150200250 300-380 400-450 _500_ 860 ‘22:40 72.60 22.80 23.00 30902.D GCMS0103.M Thu Jan 10 15:55:44 2002 Page 7 NYC-WTC_000017628

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NYC-WTC_000017628Source: NYC Law Department, mirrored locally

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Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.

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GCMS reference scan results · Box DEP Box 16

NYC-WTC_000017537

Laboratory report listing quantitative results for numerous organic compounds in a GCMS reference scan of sample AD30605 on January 9, 2002.

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