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GCMS analysis report for sample AD30902, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis identifying other unknown compounds in sample AD30902 on January 18, 2002.

NYC-WTC_000017615–000017629

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017627
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NYC 9/11 Public Portal Document . Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JANO802\30902.D Vial: 20 Acq On : 9 Jan 2002 7:51 am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table . Library : C:\DATABASE\NBS75K.L JES ISHII OI ISIS ISIS IG ISIS TODS IOS TOE ISS IE ISI IO ISOIS EI GSIO CICS IS ION I IO IC Peak Number 6 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 5 R.T. _ EstCone Area Relative to ISTD R.T. 20.86 1.46 ug/l 486572 Acenaphthene-d10 20.39 Hit# of 5 Tentative ID MW MolForm cas# Qual Benzgic acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 96 2 BepZenepropanoic acid, 4-methoxy-, 194 C11H1403 015823-04-8 43 ‘ 3 1/Butanone, 1-(4-hydroxypheny1) - 164 C10H1202 001009-11-6 38 4 £-Pentanone, 1-(4-hydroxyphenyl)- 178 C11H1402 002589-71-1 38 (Abundance San 1722 (20.886 min): 30902.0 () m/z 120.9) 100.00 | | 000. 149 ' 6 138 194 eo fw Sam ‘0, Se ales Fs S| m/z 149.00 47.52% iz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Ria See Pee 26, Fath ty eter . ii i | 149 | 138 494 20.60 _20.80_21.00_21.20 | or 68 *3 16 m/z 194.0, 27.46! fre 20_30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 | indance #21262, Benzeneoropanoit acid, 4-methoxye, methyl ester | 124 | | |_20l60 20:80 _21°00_21'20 | | 8000: [m/z 138.0, 26.99 | tes 194 |e 108. 151 183, a ->__ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 (Abundance #13456: 1-Butanone, 1-(4-hydroxyphenyl | | 181 '20.60_20.80_ 21.00 21.20 | m/z 64.9) 20.20 | 8000. | 6 Ey 2 53 nm jumare 164 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.60 20.80 21.00 21.20 30902.D GCMS0103.M Thu Jan 10 15:55:38 2002 Page 6 NYC-WTC_000017627

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NYC-WTC_000017627Source: NYC Law Department, mirrored locally

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