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GCMS analysis report for sample AD30902, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis identifying other unknown compounds in sample AD30902 on January 18, 2002.

NYC-WTC_000017615–000017629

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017626
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NYC 9/11 Public Portal Document : Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\30902.D Vial: 20 Acq On : 9 Jan 2002 7:51 am Operator: 209 GALOS Sample : goms scan 12/20a Inst : GC/MS 209 Mise : Multiplr: 1.00 Ms Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K. 1 even Sunrrrrersererterreeseetererer rrr Sl llrrrcr ttre rrrrerr rrr r tor Peak Number 5 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 3 R.T. BstCone Area Relative to ISTD R.T. 20.13. 1.77 ug/L 591089 Acenaphthene-d10 20.39 Hit# of 5 ‘Teftative ID MW MolForm cas# Qual 1 3-Isopropoy¥-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 — 071579-69-6 38 2 Trisiloxgfe, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 36 3 4-Amino-imidazole carboxamide, tr 342 C13H30N40Si3 000000-00-0 22 4 Silane/ [bicyclo[4.2.0locta-3,7-die 282 C14H2602Si2 __036461-33-3 9 Abundance Scan 1643 (20-130 ming 309020 ¢) m/z "| 100-008 S000: 147 281 327, 4s 221 as ‘9180 20,00 20120 20.40 Baa ae m/z 147.00 35.828 miz>__§0 _100__180__200 _250 _300__350_400_450__500__ 560 “Abundance % "#60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim . | 5000: i | i 147 ‘19,80 20.00 20.20 20.40 | m/z 281.00 35.42% mz» "30 100150. 200" 250 a0 350 40048050050 nares FSusGa Taslowhe, LTS £ Showatreliys SUR eT mgr | 281 ‘19180 20/00 "20.20.2040 | 8000: w/z 326.90 14.04% 369 207 249 | 338 l2n> 50 100 150 200-250 300350400450 500550 sundance #48317: 4-Amino-5-imidazole carboxamide, tis(timethyislly 5 19.80 20.00 20.20 20.40 | m/z 282.00 10.178 aor 5000. ! 237 | | , | | Wi7o 212 | 30902.D GCMS0103.M Thu Jan 10 15:55:33 2002 Page 5 NYC-WTC_000017626

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NYC-WTC_000017626Source: NYC Law Department, mirrored locally

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