NYC 9/11 Public Portal Document
_ Library Search Compound Report
. Data File : M:\INSTRU~1\209\DATA\DEC2701\30604.D Vial: 34
Acq On : 28 Dec 2001 10:13 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/17 Inst. : GC/MS 209
Misc : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
peerrrerrrrrrerrere: tester rrrrrrrrrertrt (i ttttttrttt rt ttt ttt ttt r tier ry
Peak Number 5 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 3
R.T. EstCone Area Relative to ISTD R.T.
20.28 1.31 ug/l 452670 | Acenaphthene-d10 20.56
Hit# of 5 Tentative ID MW MolForm cas# Qual
1 3-Isopropoxy-1,4,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 42
2 Trisiloxane, 1/1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38
3 4-Amino-5-imjAazole carboxamide, tr 342 C13H30N40Si3 000000-00-0 22
4 Phosphoric gid, 3-(ethoxyimino)-2- 429 C14H36NO6PSi3__055334-96-8 10
Rourdarce ‘Sean 1659 (20.277 miny: 30604.0 C) m/z 73.00 100.00%
i 47 281
ay :
i 45 221 415 20.00 20.20 20.40 20.60
' “ak te oe m/z 147.00 35.08%
oe 50100 __150 _200 _250 _300 350 _400__450 500 __550_|
peunsencs ‘#60503: Fisopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim
|
a 147 "20100 "2012020140 20:60
[m/z 281.00 31.62
a
joa 50. 100 _150 200 _250 _300 _350 450 500 550
indance i ae Trsiloxane, 7,1,1.5,5,5-hexamethyl-3,3-bis|{trimet
| | i Zet 20.00 20.20 20.40 20.60
| 8000 | m/z 326.90 12.324
| 207 249 338 id
sapere pee ee epee
Vz——> 50. 100__150 200 250 300 350 400 450 500 550
mas ‘#48317: 4-Amino-S-imidazole carboxamide, wis(timethyisily
20.00 20.20 20.40 20.60
j m/z 282.00 9.28)
i aor
5000:
237
45
| iki? 212, 1
mz->___0_100_150_ 200 _ 250300 350 _400_450_500_580 20.00 20.20 20.40 20.60
30604.D GCMS0103.M Thu Jan 10 15:04:33 2002 Page 5
NYC-WTC_000017168
OCR can misread numbers and units. Confirm readings against the page image before using them.