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GCMS analysis report for sample AD31022, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.

NYC-WTC_000017595–000017614

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017607
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31022.D Vial: 21 Acq On : 9 dan 2002 9:49 am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Prereeererrrrrrerertr rr rrrrtrrrrrtrttrrrt ltt i ttt ict tri t ttt tcrt ice t eed Peak Number 6 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 20.85 2.15 ug/1 704184 Acenaphthene-d10 20.39 Hit# of 5 Tentative ID MW MolForm cas# Qual Benzoic Acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 96 2 Benzoié acid, ethoxy-, ethyl ester 194 C11H1403 075333-22-1 43 3 1-Peyfanone, 1-(4-hydroxyphenyl)- 178 C11H1402 002589-71-1 43 _4 Benfoic acid, 2-hydroxy-, hydrazide 152 C7H8N202____—_—(000936-02-7 43 ‘Abundangé Bem 722 CORRBO ming S1GLZD G) m/z 120.9) 100.00: 5000. 149 fe 138 194 ® 69 ee 18 ay "20.60 20,80 21,00 21.20 | m/z 149.00 47.25 miz—>___20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ‘Abundance #21260: Benzolc acid, 4-ethoxy-, ethyl ester ' 11 : \ | i 149 | iia 20.60 _20.80 21.00 2120 | 438 jos | -20.80_20.80 | a 65 3 166 “ [m/z 138.05 26.51 En > 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 2 Se Se ee ee a W2I2AB: DonzOIe 30, clnoxy-, cthyl ester i 121 | | "20.60 20.60 _21,00_21.20 lp om 198 ton | = 194-0 26.25) | 29 65 es * 149 | | | | 168. vz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 | undance ‘#17210: 1-Pentanone, 1-(4-hydroxyphenyl)- ore 134 20.60 _20.80 21.00 _21.20 m/z 65.0 20.59 | 5000- if 3 53 7 ee 163. biz->___ 2030 40.50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ‘20.60 20.80 21.00 21.20 31022.D GCMSO103.M Thu Jan 10 16:07:21 2002 Page 6 NYC-WTC_000017607

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NYC-WTC_000017607Source: NYC Law Department, mirrored locally

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