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GCMS analysis report for sample AD31022, Jan 2002

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Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.

NYC-WTC_000017595–000017614

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017606
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31022.D Vial: 21 Acq On : 9 dan 2002 9:49 am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Se EESTI SSI IEE F III IIIT III IIIS OI ISI IOI III IO III AI ASIA Peak Number 5 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 3 R.T. | EstCone Area Relative to ISTD R.T. 20.12 2.93 ug/1 957402 Acenaphthene-d10 20.39 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 3-Isopropoyy~1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 45 2 Trisiloxpfe, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37 3 Octadegénoic acid, 2-[(trimethylsil 386 C22H4603Si 056196-58-8 10 4 Phosphoric acid, 2-(methoxyimino) -3 415 C13H34NO6PSi3__055319-85-2 9 Rbundance ‘Scan 1643 (20.125 min): 31022.D (-) m/z 73.00 100.00 | ‘5000 ' “wr 281 | y i 45 21 eis 415 49.80 20.00 20.20 20.40 i Se ree eneeran 205 20 peepee m/z 147.00 35.72 fniz->__ 80 100__180__200_250__300__350_400_450_500_ 560 Abundance #50803: Slsopropony-1,1,1,7,7,7-hexamethyl-3.5.6-tis(vim t : | roe at 147 Tz 20.00 20.20 20.40 m/z 281.00 31.32 1B ; | 1 sar “15 519 561 muz->___" 60.100 __150__200 _280 _900__350_400__ 480__ 500 _580 Woundancé———S*C*SZSO: Trisloxane, 1,171.5.5.5heamedy-3.s-be\(timmot | 7 147 | 281 19:80 20.00 20.20 20.40 5000 | m/z 326.9 11.98 i | ea | 207 249 338 | > 80-100 150-200-250 300350 _400__ 450 _500 _§50 undance Tn FTa26; Ociadecanolc 66d, 2[rimethysliyog, methyl —r7 19.80 20.00 20.20 20.40 ¥ 327 m/z 282.00 8.78 5000: . 103129 459 i miz—> 0100150 200-250-300 300-400 450 500580. 49.80 20.00 20.20 20.40 31022.D GCMS0103.M Thu Jan 10 16:07:15 2002 Page 5 NYC-WTC_000017606

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NYC-WTC_000017606Source: NYC Law Department, mirrored locally

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