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GCMS analysis log for sample AD30634

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30634 performed on January 22, 2002.

NYC-WTC_000017299–000017319

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017310
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NYC 9/11 Public Portal Document : Library Search Compound Report . Data File : M:\INSTRU~1\209\DATA\DEC2701\30634.D Vial: 28 Acq On : 28 Dec 2001 4:21 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K. 1 JESS ISITE IE IS ISS IOI IO IS IIS ICIS ISOS E ICIS ISTIC IS ISU IO Peak Number 5 Benzoic acid, 4-ethoxy-, ethyl Concentration Rank 12 R.T. EstCone Area Relative to ISTD R.T. 21.04 1.02 ug/l 503421 § Acenaphthene-d10 20.56 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Benzoi¢ acid, 4-ethoxy-, ethyl este 194 C11H1403 023676-09-7 96 2 Ethylfaraben 166 C9H1003 000120-47-8 53 3 Ethghone, 1-(4-ethoxyphenyl) - 164 C10H1202 001676-63-7 42 4 Bepfzoic acid, 2-hy -, hydrazide 152 C7H8N202 000936-02-7 38 ae ‘Bean 1742 GA. 087 min}: S064 DG) m/z 120.95 100.00 e000. 149 | id 93 we 166 “ i Bo | 7 20.80 21.00 21.20 21.40 | re 1 m/z 149.00 49.38 > 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Feta gcg 00-80. ae oo 00 W2iab0: Benzke etd, etn, ethyl ester | | 10 if bana 20.80 21.00 21 21.40 499) y y | n ie Pi 18 ‘* [m/z 194.05 28.17 = 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 indance #IGG54. Ethyiparaben | cr 20.80 21.00 21.20 21.40 | 8000: | m/z 138.0) 24.55) | 65 93 | 138 166 5 | | | > 20-3040 80. 60 70 80. 90 100 110 120 10 140 160 100 170 160 100 200, | sundance: ‘#1315: Ethanone, 1-(4-ethoxyphenyl}- | 121 20.80 21.00 21.20 21.40 | Wn) m/z 65.05 19.53 i 5000. | 85 93 164, | ar ae 107 . Saad 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.80 21.00 21.20 21.40 30634.D GCMS0103.M Thu Jan 10 14:09:52 2002 Page -5 NYC-WTC_000017310

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NYC-WTC_000017310Source: NYC Law Department, mirrored locally

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