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GCMS analysis report for sample AD31022, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.

NYC-WTC_000017595–000017614

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017609
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31022.D Vial: 21 Acq On : 9 Jan 2002 9:49 am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Perrewrrerrrrrrrrer rere rerrrrrrerterrrttr rrr tilt irri tri i iti t torre roy Peak Number 8 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 7 R.T. | EstConc Area Relative to ISTD R.T. 26.73 0.81 ug/l 269920 Phenanthrene-d10 24.81 Hit# of 5 Tefitative ID MW MolForm cas# Qual 1 3-IsopropeéKy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 50 2 Trisilpxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 42 3 Ethapédioic acid, bis(trimethylsily 234 CeHiso4si2 018294-04-7 32 4 Mandelic acid dithdms __—_—_—_—_—'380_C20H3603Si2_ __078324-07-9 27 Roundancs ‘Scan 2363 (26.734 rink 310220 () m/z 73.00 100.008 i} 5000: i 147 21 (at secre oer | “s 385 429 26.40 26.60 26.80 27.00 | Woche Bote Bit rer [m/z 147.00 34.06 Abundance ‘#60503: 3-isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim it / | | 5000- | 147 ie 26.60_26.80_ 27.00 i m/z 281.00 16.61 i 1 VZ—> 50 400 __150 200 250 300 3650 400 450 500 550 | andanes aes Tristoxane, 1,1.1,5.5,5-hexamethy-3,3-bisi(timet | 1 | j i T V | i cd | 28.40 _26.60_26.80_27.00 50004 i m/z 221.0 16.14 i { | | : | i 369 | 1 | L207 249, 338_| bntan> ‘30100150200 250. 300350 400 450500. 550 | ‘Abundance #30680; Ethanedioic acid, bis(trimethylsily)) ester_ { ss 28.40 _28.60 26.80 _27.00 | m/z 207.00 7.88 : | 5000: | 45 | 190 219 mize 50 100 150 200 280 300 350 400 450 500 550 2640 26.60 26.80 27.00 31022.D GCMS0103.M Thu Jan 10 16:07:32 2002 Page 8 NYC-WTC_000017609

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NYC-WTC_000017609Source: NYC Law Department, mirrored locally

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