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GCMS analysis report for sample AD31022, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.

NYC-WTC_000017595–000017614

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017610
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NYC 9/11 Public Portal Document . . Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31022.D Vial: 21 Acq On : 9 dan 2002 9:49 am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L eeerewrerrrrrrrrer rrr rrrrrrrrrrrrrrtr ii ri rrrrr rrr irri re rire rolls Peak Number 9 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 11 R.T. | EstConc Area Relative to ISTD R.T. 28.50 0.58 ug/1 191379 Phenanthrene-d10 24.81 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 3-Isopropoxy‘1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 2 1-Monolineleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 36 3 Benzoip“acid, 2,4-bis[(trimethylsil 370 C16H3004Si3 010586-16-0 25 4 _N-(Tyffluoroacetyl) -N,0,0',O''-tetr 553 C22H42F3NO4Si4 000000-00-0 12 Roundancs, ‘Scan 2655 (28.497 miny: 31022. (-) m/z 73.00 100.00 | | | i 5000: | 147 | 21 og, 358 28.20 28.40 28.60 28.80 | | 45 117, 191; | 249 327 401,429 ae 147-10 33.629 bniz-> 50 100 150 200 250 300 350 400 450 500550 (Abundance '#60503: 3-isopropoxy-1,1,1,7,7,7-hexamethyl-3.6,Stris(tim . | | | 147 2820 28:40 28.60 2880 m/z 221.0, 19.55% 21-281 aor Fr of sot > ‘30 100150 200 250° 300 350 400 450 500850 | undance #SBETT: |-Monolinolooyigiycora rindi yisiy ether | if 3 | | 207 28.20 28.40 28.60 28.80 | sooo wr 8 m/z 355.0 16.80% | 34 103 ! | 281 | | | ee 482 mz> "80100150200 250 300 360 400450500 _500_| ‘Abundance #73875; Benzoic acid, 24-bie[(timethyisiiyjoxyp, timet | a | 28.20 28.40 28.60 28.80 i | m/z 281.0) 14.56 i : | 5000: 355 | 45 | | 193493. 223281 miz—> ‘50100 150 200 250 300 350 400 450 500 550 ‘28.20 2840 2860 28.80 | 31022.D GCMS0103.M Thu Jan 10 16:07:38 2002 Page 9 NYC-WTC_000017610

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NYC-WTC_000017610Source: NYC Law Department, mirrored locally

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