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GCMS analysis results for sample AD30633, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.

NYC-WTC_000017210–000017232

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017226
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\30633.D Vial: 27 Acq On : 28 Dec 2001 3:23 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 3-Isopropoxy-l, 1,1,7,7,7-hexam Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 28.66 1.15 ug/1 550987 Phenanthrene-dl0 24.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-X,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 37 2 Trisiloxane,/l,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 35 3 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 25 4 N-(Trifluoroacetyl)-0,0',0'1-tris(t 481 C19H34F3NO4Si3 000000-00-0 25 Abundance Scan 2572 (28.659 mln): 30633.D (-) m/z 73.00 1 00.00% 73

5000 147 221 281 355 .. 249 [ 327, 401429 28.40 28.60 28.80 29.00 ■ 45 1 r 117 1 *i , 191 f* Pi .). Pi* । m" ;■ । f. 111 .. । 11 i । । 11 11 m/z 147.00 36.58% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 ...... / V....... 147 28.40 28.60 28.80 29.00 221 281 20- A4E m/z 355.05 22.58% , I... I . , J, 1... 415.... 519 , 561 m/z-> 50 100 150 200 250 300 350 400 450 ' 500 550 ' Abundance #52459: Trisiloxane, 1,1.1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 281 28.40 28.60 28.80 29.00 5000 rn/z 221.05 22.03% 369 207 249, j 338 | • . • । ‘ > ■ ■ i ' • 1 •i■•■■I11111'1 f 1 I ' ' 1 1 1 1 ■ ■ i• • ■ rl 1 ' '1 I 1 1' ' I 1 1 miz-> Abundance 50 100 150 200 250 300 350 400 450 500 550 #73978: Benzoic acid, 2,5-bis(trimethylsiloxy), trimethyls ... A.... 73 28.40 28.60 28.80 29.00 355 m/z 281.00 17.45% 5000 45 147 179 223, 267 297 ‘ ' I • • ■ ‘ I ' 1 1 1 I 1 1 ' 1 I 1 1 1 ‘ I ‘ 1 ■ ■ i ■ ■ 1 • i ■ • 1 1 i ' 1 1 1 i ' • m/z~> 50 100 150 200 250 300 350 400 450 500 550 28.40 28*60 28.80 29.00

30633.D GCMS0103.M Thu Jan 10 15:24:24 2002 Page 10

NYC-WTC_000017226

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NYC-WTC_000017226Source: NYC Law Department, mirrored locally

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