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GCMS analysis log for sample AD30608

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.

NYC-WTC_000017192–000017209

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017202
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NYC 9/11 Public Portal Document = Library Search Compound Report : Data File : M:\INSTRU~1\209\DATA\DEC2701\30608.D Vial: 32 Acq On : 28 Dec 2001 8:16 pm . Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L TEI ISIS SSIES SSSI ISIS SIG ISH ISEI SIO IS ISS ISEIOG IG SIG SEIS IS Inn toi iniior Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 2 R.T. EstCone Area Relative to ISTD R.T. 17.45 3.01 ug/l 1193220 Naphthalene-ds 15.28 Hit# of 5 Tentative zD MW MolForm CAS# Qual 1 Cyclohexasiloxane, Aodecamethyl- 444 C12H3606Si6 000540-97-6 38 2 4-Amino-5-imidazo¥e carboxamide, tr 342 C13H30N40Si3 000000-00-0 32 3 1,1,1,5,7,7,7-Hoptamethyl-3,3-bis(t 444 C13H4005Si6é 038147-00-1 25 4 2H-1,4-Benzodig¢zepin-2-one, 7-chlor 342 C18H19CIN20Si _055299-24-6 12 Foundance ‘Sean 1351 (17.450 min: 30608.D (-) m/z 72.95 100.00 5000: i at 147 | 45 . ean 429 417.20 17.40 17.60 17:80 | 97 117 179 20795 251 261 311 ec aye al 6 OLE mmiz—>__ 40 60_80 100 120 140 160 180200 220 240 260 280 300 320 340 360 380 400420 (Abundance ——~=—~=~S*S*«RS G11: Cyclohexasloxane, dodecamethyi- | | | at | | 429 | 5000 | 17.20 17.40 17.60 17.60 | 147 m/z 147.00 13.45: i a7 | 207 267 344 bvz—> 40.60 _80_ 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380400 420 . Abundeneg 7p es amin Samal carboraT Ce, HEINE Ny | 327 47.20_17.40_17.60 17.80 ‘5000. | m/z 342.0, 9.61 | | 237 5 | i | ‘47 472 212 | 255 | => __ 40 60 _80 100 120 140 160 180 200 220 240260 260 300 320 340 360 380.400 420 dance #56714: 1,1,1,5,7,7,7-Heplamethy:3,3bis(timethyislioy)t 1 17.20 17.40 17.60 17.80 m/z 325.0, 9.48% 147 | 8000 267 ass ws i 45 207 Iniz-> "40 60-80 100 120 140 160 180 200 220 240 260 260 300 320 340 360 380 400 420 17.20 17:40 17.80 17.80 30608.D GCMS0103.M Thu Jan 10 15:08:06 2002 Page 4 NYC-WTC_000017202

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NYC-WTC_000017202Source: NYC Law Department, mirrored locally

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