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GCMS analysis report for sample AD31022, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.

NYC-WTC_000017595–000017614

Folder label: “GCMS X 12/20/01 A 1/9/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31022.D Vial: 21 Acq On : 9 Jan 2002 9:49 am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSE ISSI SUISSE IS IGS ISIS ISTIC IS SIIC II ICIS GEIS HIOGI SOI TOOTS TI III Peak Number 3 Cyclohexasiloxane, dodecamethy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 17.31 4.16 ug/l 1287830 | Naphthalene-ds 15.12 Hit# of 5 Tenfdtive ID MW MolForm cas# Qual 1 Cyclohexasiéxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 36 2 1,1,1,5,7/7,7-Heptamethyl-3,3-bis(t 444 C13H4005Si6é 038147-00-1 35 3 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19C1N20Si 055299-24-6 22 4 Silang, [1,2,3-benzenetriyltris (oxy 342 C15H3003Si3 017864-23-2 12 oundancs 7” “Scan 1336 (17.306 min}: 31022.D ¢) m/z 73.00 100.00 i if | 3000 : 3a 45 207 429 17.00 17.20 17.40 17.60 | i ie auesiiamen —s_- m/z 341.00 28.70% > 40 _60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360380400420 | Abundance #56711: Cyclohexasiioxane, dodecamethyl- | 3a . | 429 i | 17.00 17:20 17.40 17.60 ! 147 m/z 147.00 14.15 | A17, 207 267 att i} mz 40_60_80 100 120 140 160 180200 220 240 260 280 300 320 340 360 380 400.420 alana ~ HS6714°1.1,1.5.7,7,7-Heptamethy-3.s-bis(tnmethyisiiony | i i i 447 17.00 17.20 17.40 17.60 ‘a0 | 287 m/z 325.00 10.14 | 355, 429 a | 207 | ' | ————— imz—>_ 40_60_80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380400 420 ‘Abundance #48337: 2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- i ‘17.00. 17:20 1740 17.60 | [m/z 342.00 9.95 5000: | 45 a i 116 148 2 269 a5 ‘miz->__” 4060. 80.100 120 140 160 180 200 220 240 260 260 300 320 340 360 380 400 420 17.00 17.20 17.40 17.60 31022.D GCMS0103.M Thu Jan 10 16:07:03 2002 Page 3 NYC-WTC_000017604

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NYC-WTC_000017604Source: NYC Law Department, mirrored locally

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Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.

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