Laboratory report documenting GCMS analysis of sample AD31023 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
NYC-WTC_000017630–000017648Folder label: “GCMS X 12/20/01 A 1/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File M:\INSTRU~1\209\DATA\JAN0802\31023.D vial: 25 Acq On 9 Jan 2002 1:44 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
17.31 2.99 ug/1 1015200 Napht halene-d8 15.13
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasilo: me, dodecamethyl- 444 C12H3606Si6 000540-97-6 45 2 1,1,1,5,7,77 -Heptamethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 23 3 2H-1,4-Be:nzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 4 Silane, A 1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12 Abundance ( Scan 1336 (17.312 min): 31023.D (-) m/ z 73.00 100.00% 73
5000 341 ,... 147 429 17.00 17.20 1740 17.60 ' 45 । miz-> 0- mmkm —————I — ——117 179.207225 251 281 311 [ t 397 40 60 80 100120140160180200220240260280300320340360380400420 1 m/z 341.00 34.01% Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 5000 17.00 17.20 17.40 17.60 m/z 147.CO 14.15% 147 I 207 267 | 311 [ [ 117 TumempnmuBu*u]—]mn—umpun—u‘TTTpTTrpTTTpTTTprrrp- m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714: 1.1.1.5,7.7.7-Heptamethyl-3.3-bis(trimethylsiloxy)t 7)3 P 17.00 17.20 17.40 17.60 147 5000 267 m/z 325.00 11.49% 355 429 45 207
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48337:2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 73 341 17.00 17.20 17.40 17.60 m/z 342.00 11.37% 5000 45 91 I 116 146 227 299 315 I Tnmnpmmgmmgmammp TTpp m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 17.00 17.20 17.40 17.60
31023.D GCMS0103.M Thu Jan 10 16:11:46 2002 Page 4
NYC-WTC_000017640
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NYC-WTC_000017571
Laboratory report documenting GCMS analysis of sample AD30903 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017595
Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017556
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31019 performed on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017542
Laboratory report documenting GCMS blank analysis for volatile organic compounds on sample AD30605 conducted on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017615
Laboratory record of GCMS analysis identifying other unknown compounds in sample AD30902 on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017246
Gas chromatography-mass spectrometry analysis report for sample AD30602 showing detection of 2,4-DDD and other unknown compounds, analyzed January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017171
Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017210
Laboratory report documenting GCMS analysis of sample AD30633 including DDD surrogates on January 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018005
Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018882
GCMS analysis report for sample AD30488 showing detection of unknown compounds and surrogate recovery data from February 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000017529
Document page containing no readable text or identifiable content for description purposes.
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NYC-WTC_000017530
Unreadable document containing GCMS analytical data from the Department of Environmental Protection dated January 2002.
Filed in the same folder
NYC-WTC_000017533
Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.
Filed in the same folder
NYC-WTC_000017537
Laboratory report listing quantitative results for numerous organic compounds in a GCMS reference scan of sample AD30605 on January 9, 2002.
Filed in the same folder
NYC-WTC_000017542
Laboratory report documenting GCMS blank analysis for volatile organic compounds on sample AD30605 conducted on January 10, 2002.
Filed in the same folder