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GCMS analysis report for sample AD31022, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis for unknown compounds in sample AD31022 conducted on January 18, 2002.

NYC-WTC_000017595–000017614

Folder label: “GCMS X 12/20/01 A 1/9/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\31022.D Vial: 21 Acq On : 9 dan 2002 9:49 am Operator: 209 GALOS Sample : gems scan 12/20a Inst. : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Prenenwtamnernrrrrerrererrrrrrrrrrrrrrrrro rr’ 2 ltr h ttt eta aad Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 5 R.T. | EstConc Area Relative to ISTD R.T. 14.17 1.97 ugf 610882 § Naphthalene-ds 15.12 Hit# of 5 entative ID MW MolForm cas# Qual 1 Cyclopentésiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Benzoic Acid, 2,6-bis[(trimethylsil 370 C16H3004Si3 003782-85-2 50 3 Benzoic/acid, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 47 4 _N-(Trifluoracetyl) -0,0',O"-tris (tri 495 C20H36F3NO4Si3_ 000000-00-0 47 ‘Abundance ‘Scan 994 (14.167 miny: 31022. () m/z 72.9) 100-00 | | 1 5000: i a | 45 184177193 293-254 323339 13.80_14.00 14.20 14.40 oO 2 errr rt i A wa | m/z 267.00 32.37 imi 40.60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiioxane, decamethyl- 355 | | 5000: ar | |Seecz j | | 43.80. 14,00 14.20 14.40 | | m/z 355.0 23.56% | 491207 254 323339 | ivz->__ 40 60_80_100 120 140 160 180 200 220 240 260 280 300 320 340 360_ | ‘Abundance 51206, Benzole acid, 26-bsirimettysiyory} vamet— | 355 i oe | 13.80 14.00 14.20 14.40 | 6000 m/z 268.00 8.90 | i | 147 287 i 47 208249 | 283 370 |niz-> _"W0'"G"”'8O 100.180 140 160 160.200 280 240 260 260 300 320 340.360 ‘Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy}, trimethyls oe aaron | 43.80 _14.00 14.20 14.40 i 385 [m/z 356.0 8.58) | 5000: 45 147479207223 2679 370 fa 40.60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 43.80 14.00 14.20 14.40 31022.D GCMS0103.M Thu Jan 10 16:06:57 2002 Page 2 NYC-WTC_000017603

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NYC-WTC_000017603Source: NYC Law Department, mirrored locally

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