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GCMS analysis report for sample AD30902, Jan 2002

Machine-extracted title · confidence 95%

Laboratory record of GCMS analysis identifying other unknown compounds in sample AD30902 on January 18, 2002.

NYC-WTC_000017615–000017629

Folder label: “GCMS X 12/20/01 A 1/9/02

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Scanned page image, NYC-WTC_000017624
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\JAN0802\30902.D Vial: 20 Acq On : 9 Jan 2002) 7:5] am Operator: 209 GALOS Sample : gems scan 12/20a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT|P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NB$75K.L eereerrrrerrrrererrsstrrererer Setrtrrtrrrrtttrttt rt titi ttt tr rit ttry Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 4 R.T. EstCone Area Relative to ISTD R.T. 14.17 1.56 ug/1 50032 Naphthalene-ds 15.13 Hit# of 5 Tehtative ID MW MolForm cas# Qual 1 Cyclopentag4loxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 Benzoic afid, 2-[(trimethylsilyl) ox 282 C13H2203si2 003789-85-3 47 3 Benzenegthanamine, N-[(pentafiluorop 475 C21H26F5NO2Si2 055429-85-1 38 4 Benzoid acid, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 35 ‘Abundance a ~ Sean 804 (14.172 min): 39902. m/z 73.00 100.00: | 8000: ar 358 1 45 193. 251 413.80 14,00 14.20 14.40 14.60 i L. 88 103118133 154 177 298223 293 323339 m/z 267.00 38.13! > 40 60 80 100 120 140 160 180 200 220 260 280 300 320 340 360 ovens +#51266! Cyclopentasiioxane, Hecametiy- | | | ar | |—ee | bepeerey i eee | [[aaleo'taloo"“14:20"‘ta40. 14.60 | | [i/z 385.05 "28.03 | 191 207 251 323339 | jmiz->___ 40 _60_80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ‘Abundance #72208; Benzoic acid, 2-{(trimethyisily)joxy)-. timethyisi { 7p 267 } | : 13.80 14.00 14.20 1440 14.60 | 8000: | le z 356.05 10.01) : 135 193.209 i bwz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74573: Benzeneethanamine, N-{(pentafiuorophenyljmethyiene] ore 1 13.80 14.00 14.20 14.40 14.60 i m/z 268.00 9.75! | 5000: ii | 267 | 44 | | | 151 179194209 250 | mz-> 40-60 _80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 | 13.80 14.00 14.20 14.40 14.60. 30902.D GCMS0103.M Thu Jan 10 15:55:21 2002 Page 3 NYC-WTC_000017624

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NYC-WTC_000017624Source: NYC Law Department, mirrored locally

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