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GCMS analysis log for sample AD30634

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30634 performed on January 22, 2002.

NYC-WTC_000017299–000017319

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017308
OCR text

OCR status: ocr · source: ours

NYC 9/11 Public Portal Document . Library Search Compound Report : Data File : M:\INSTRU~1\209\DATA\DEC2701\30634.D Vial: 28 Acq On : 28 Dec 2001 4:21 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L FEISS IG GSI IGG IOI EI ICI ISITE IIIT IOI ICICI III III IIIT : Peak Number 3 Cyclohexasiloxane, dodecamethy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 17.46 5.37 ug/l 2418980 Naphthalene-d8 15.28 Hit# of 5 mtative ID MW MolForm cas# Qual 1 Cyclohexasgfloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 45 2 2H-1,4-Befzodiazepin-2-one, 7-chlor 342 C18H19CIN20Si 055299-24-6 12 3 1,1,1,5,,7,7-Heptamethyl-3,3-bis(t 444 C13H4005si6é 038147-00-1 12 4 Silane /[1,2,3-benzenetriyltris (oxy 342 C15H3003Si3 017864-23-2 10 ‘Abundance “Scan 4352 (17.457 miny: 30634. (-) m/z 73.00 100.00% i i | 5000. 344 147 429 | 45 207, | __17.20_17.40_17.60_17.80__| \ ian Pa inSain tt in m/z 341.00 36.93 . niz>___40_60_80 100 120 140 160 180200220 240 260 280 300 320 340 360 380 400420 ‘Abundance #56711: Cyciohexasiloxane, dodecamethyl- | He at a | 429 | i | | ‘1720 1740 1760 1780 | i 147 m/z 147.00 14.87% a7 | 207 ort | = 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360380400420 Abundance *BA8I37: DH-T 4-Benzodiazopin-2-one, 7-chioro- 1, 3-dihyaro-s | ® | | 17:20 17.40 17:60 17.80 5000: { | m/z 429.0) 12.30 | 4 | ot | | | 16 146 27 9 os | ener beeper ere nprnp ere ep he Pee TT TTT aa 40 _60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400420 indanca: #56714: 1,1,1,5,7,7,7-Heptamethy/-3,3-bis(timethyislioxy)t 47.20 _17.40_17.60_17.80 | m/z 325.00 12.10 | 147 1 5000- 267 355 43 207 “ od 40 _60_80 100 120 140 160 180 200220 240 260 280 300 320 340 360380400 420 17.20 17.40 _17.60_17.80 30634.D GCMS0103.M Thu Jan 10 14:09:40 2002 Page 3 NYC-WTC_000017308

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NYC-WTC_000017308Source: NYC Law Department, mirrored locally

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