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GCMS analysis log for sample AD30634

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30634 performed on January 22, 2002.

NYC-WTC_000017299–000017319

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017307
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OCR status: ocr · source: ours

NYC 9/11 Public Portal Document ., Library Search Compound Report . Data File : M:\INSTRU~1\209\DATA\DEC2701\30634.D Vial: 28 Acq On : 28 Dec 2001 4:21 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Preerretrrrrrrrrrr rr fSrrrerrrrrrrrrrrtrr rrr tert ttt irre ttt tert tte retry Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 5 R.T. _EstCone Area Relative to ISTD R.T. 14.31 1.61 ug/1 727848 Naphthalene-d8 15.28 Hit# of 5 ‘entative ID MW MolForm cas# Qual 1 Cyclopenfasiloxane, decamethyl- 370 C1OH3005Si5 000541-02-6 72 2 Benzoico/acid, 2,6-bis[(trimethylsil 370 C16H3004Si3 003782-85-2 40 3 3,4-Difydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38 4 Benzofic acid, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 37 Poundence ‘Scan 1009 (14.308 min: 30634.D (-) m/z 73.00 100.004 | i 5000: i ar 355 45 193, 254 14.00 14.20 14.40 14.60 i 89 108 133 154 177 1982 293 323339 m/z 267.00 36.31 > 4060 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360. ir ie #51206: Cyclopentasiioxane, decamethyi- i 355 | 000 7" i | ‘14.00 14.20 14.40. 14.60 j i m/z 355.0) 27.91% | 491207251 323330 fvz—>___40_60_80_100 120 140 160 180 200 220 240 260 260 300 320 340 360 (Abundance #51295: Berizoic acid, 2.6-bis|(trimethyisily joxy]-, rimet ee | i | sarge ar | 5000 m/z 356.0 10.11: 17 ar t a7 I 208 249283 | 370 Iniz->____ 4060 _80_100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance *#49868: 3 4-Dihydroxybenzyl alcohol. is(timethyisliyi- i 14.00 14.20 14.40 14.60 | m/z 268.00 9,17 | 267 | sooo | 179 356 | 2 147 | | crrtherprersherer ee 38t rep Br three, miz->__40_60_80 100 120 140 160 180 200 220 240 260 260 300 320 340 360 14.00 14.20 14.40 14.60 30634.D GCMS0103.M Thu Jan 10 14:09:34 2002 Page 2 NYC-WTC_000017307

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NYC-WTC_000017307Source: NYC Law Department, mirrored locally

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