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GCMS analysis log for sample AD30603

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD30603 on January 22, 2002.

NYC-WTC_000017233–000017245

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017241
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NYC 9/11 Public Portal Document a Library Search Compound Report . Data File : M:\INSTRU~1\209\DATA\DEC2701\30603.D Vial: 31 Acq On : 28 Dec 2001 7:17 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L FEISS OSI ISIS IETS II HISIG SIGE IG ITSO IOI IOI IIT TIO III Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 5 R.T. _ EstCone Area Relative to ISTD R.T. 14.31 0.47 ug/l 241095 Naphthalene-ds 15.28 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Cyclopentagfloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Benzoic agMd, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 38 3 3,4-Dihygfoxybenzyl alcohol, tris(tr 356 C16H3203Si3 068595-79-9 37 4 Benzoic Acid, 2,6-bis|(trimethylsil 370 C16H3004Si3 003782-85-2 33 Rbundance ‘Sean 1009 (14.305 min}: 30603.D ¢) m/z 73.00 100.008 i | | 5000: er 355 45 193, 251 14.00 14.20 14.40 14.60 | 493 133 154 177193 298 323930 az 266-5) PERT >" A) 60 80 100 120 140 160 180 200 220 240 260 280 300 320 poe *¥51266: Cyclopentaslioxane, decamethyl- | | 355 | 267 | 000. ; | 00120 1440 Geo | \ m/z 355.0, 24.33 251 339 wmiz—>_ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360. undance ‘#75978; Benzoic ecid, 2.5-bis(timethyisiloxy}, trimethyis i a8 { 14.00 14.20 14.40 14.60 | 5000 m/z 356.0 9.39% 6 | 147479 207223 287282297 | 370 VZ-—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360. bundance ‘#49888: 3,4-Dihydroxybenzyi alcohol, tris(trimethyisllylj- | 7p 14.00 14.20 14.40 14.60 | m/z 74.00 9.35% | 5000. | 479 id | 356 45 147 209 237 312 344 miz> 40_60_ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60 30603.D GCMS0103.M Thu Jan 10 15:01:37 2002 Page 2 NYC-WTC_000017241

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NYC-WTC_000017241Source: NYC Law Department, mirrored locally

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