NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30650.D Vial: 46
Acq On : 30 Dec 2001 3:26 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/18 Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
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Peak Number 2 Benzene, l-phenyl-4-(2-cyano-2 Concentration Rank 14
R.T. EstConc Area Relative to ISTD R.T.
11.13 0.44 ug/1 203289 1,4-Dichlorobenzene-d4 11.67
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 50
2 Cyclotetrasiloxane, octamethyl- 296 C8H2404Si4 000556-67-2 25
3 2-0xo-4-phe: ^1-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9
4 6,7-Benzo-p enothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9
Abundance Scan 663 (11.132 min): 30650.D (-) m/z 281.00 100.00%
281
5000
45 59 73 89 103 119 133 147 163 177 193 207 235 249 235 10.80 11.00 11.20 11.40
TUTTTT ■ ■ i1 1 1 1 i 1 '1 Y"i ' 1 11 1 1 1 1 I ’r1 1 t"I ' 1,1 1 ■' 1 ■ ■ । ■ > • • । ■ 'I ■ । ■ ■ ■ ■ I m/z 282.00 26.98%
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260. 280
Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl)
281
5000-
10.80 11.00 11.20 11.40
203
253 m/z 283.00 17.30%
।
miz—>
। । । । । । । । । ■
40 60 80
126
I _224
■ ■ i ' ■ ' ■ i ■ ■ ■ ' i ■ ' ' ■ i ' '
100 120 140 160 180 200 220
240.4,266.1
240 260 280
(Abundance +72646. Cclotetrasiloxare, octamethyl
281
TT
10.80 11.00 11.20 11.40
5000- m/z 192.90 10.99%
265
45 59 73 133 177 193 207 235
m/z-> 40 60__ 80__ 100 120 140 160 180 200 220 240 260 280
Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi ■ ■ i ■ 1 ■ ■ l 1 ■ ■ ■ ।
281 10.80 11.00 11.20 11.40
m/z 132.90 9.25%
5000-
102 , 123 141 .......175 204 .......... 247 ......... TT
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40
30650.D GCMS1126.M Mon Jan 28 11:18:07 2002 Page 2
NYC-WTC_000004372
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