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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004372
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30650.D Vial: 46 Acq On : 30 Dec 2001 3:26 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Benzene, l-phenyl-4-(2-cyano-2 Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

11.13 0.44 ug/1 203289 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 50 2 Cyclotetrasiloxane, octamethyl- 296 C8H2404Si4 000556-67-2 25 3 2-0xo-4-phe: ^1-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 4 6,7-Benzo-p enothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 Abundance Scan 663 (11.132 min): 30650.D (-) m/z 281.00 100.00% 281

5000

45 59 73 89 103 119 133 147 163 177 193 207 235 249 235 10.80 11.00 11.20 11.40 TUTTTT ■ ■ i1 1 1 1 i 1 '1 Y"i ' 1 11 1 1 1 1 I ’r1 1 t"I ' 1,1 1 ■' 1 ■ ■ । ■ > • • । ■ 'I ■ । ■ ■ ■ ■ I m/z 282.00 26.98% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260. 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 281

5000- 10.80 11.00 11.20 11.40 203 253 m/z 283.00 17.30% । miz—> । । । । । । । । । ■ 40 60 80 126 I _224 ■ ■ i ' ■ ' ■ i ■ ■ ■ ' i ■ ' ' ■ i ' ' 100 120 140 160 180 200 220 240.4,266.1 240 260 280 (Abundance +72646. Cclotetrasiloxare, octamethyl 281 TT 10.80 11.00 11.20 11.40 5000- m/z 192.90 10.99% 265 45 59 73 133 177 193 207 235 m/z-> 40 60__ 80__ 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi ■ ■ i ■ 1 ■ ■ l 1 ■ ■ ■ । 281 10.80 11.00 11.20 11.40 m/z 132.90 9.25% 5000-

102 , 123 141 .......175 204 .......... 247 ......... TT m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40

30650.D GCMS1126.M Mon Jan 28 11:18:07 2002 Page 2

NYC-WTC_000004372

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NYC-WTC_000004372Source: NYC Law Department, mirrored locally

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