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GCMS analysis results for sample AD30601, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD30601 for volatile organic compounds on January 10, 2002.

NYC-WTC_000017126–000017138

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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Scanned page image, NYC-WTC_000017132
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : M:\INSTRU~1\209\DATA\DEC2701\LBB.D vial: 24 Acq On : 28 Dec 2001 12:26 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.61 3.77 ug/1. 1417360 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 ntative ID MW MolForm CAS# Qual 1 N-Ethyl fo: amide 73 C3H7NO 000627-45-2 9 2 1,3 -Dioxd ane. 2-methyl- 88 C4H802 000497-26-7 9 3 Pentane/ 3-methoxy- 102 C6H140 036839-67-5 9 4 1,3-Di xolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance Scan 280 (7.611 mln): LBB.D (-) m/ z 73.0,0 100.00% 73

5000 43 1 i i n । » 4 » t411 j1 j i i" । Ti r*1 87 7.20 7.40 7.60 7.80 8.00 0- ......... . ............ 38.1 1—— + • i • • » • t ‘ ‘ • i • ‘ ' • * m/z 1 50 55 60 67, 1 103 j 43.0,5 32.06% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73

5000 fl » i l pl » » I J 112‘I

58 7.20 7.40 7.60 7.80 8.00 44 m/z 45.05 11.10% 15 I i .nanlaje 1 1 4 i'I'I'I . । , i ■ ■ ‘ • i 1 1 ■ • i ■ ■ ' ■ i • ■ ■ ■ । ■ 1 ■ 1 i ■ ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902: 1,3-Dioxolane, 2-methyl 73 [4 » » r p < "" 1 j i j r • j' r 1 • i ■ ■ 7.20 7.40 7.60 7.80 8.00 5000 43 m/z 41.00 10.74% 58 27 87 ' 1 I 1 1 ‘ rp 1 1, 1’ ' ■ ■ i 1 ■ ■ 1 i ■ • ■ • i ■ ■ ■ ■ i • 1 1 ■ i ■ ■ ■ • i • • ■ ■ I ■ ■ ■ ■ i ■ ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentene, 3-methoxy- 73 7.20 7.40 7.60 7.80 8.00 m/z 71.0.0 7.34% 5000 45

. .......... . 33.39, TIIut 55 ■ ■ i • ■ • 1 I ■ • 1 ■ i ■ • ■ • i 1 • • 1 ■ • । ■ ■ ■ ■ । • i ' ■ ■ ■ i 1 ‘ 1 11 pni r ■ . m/z-> 10 20 30 40___ 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

LBB.D GCMS0103.M Thu Jan 10 13:58:29 2002 Page 1

NYC-WTC_000017132

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NYC-WTC_000017132Source: NYC Law Department, mirrored locally

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