NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : M:\INSTRU~1\209\DATA\DEC2701\LBB.D vial: 24
Acq On : 28 Dec 2001 12:26 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/17 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 1 N-Ethylformamide Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
7.61 3.77 ug/1. 1417360 1,4-Dichlorobenzene-d4 11.68
Hit# of 5 ntative ID MW MolForm CAS# Qual
1 N-Ethyl fo: amide 73 C3H7NO 000627-45-2 9
2 1,3 -Dioxd ane. 2-methyl- 88 C4H802 000497-26-7 9
3 Pentane/ 3-methoxy- 102 C6H140 036839-67-5 9
4 1,3-Di xolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9
Abundance Scan 280 (7.611 mln): LBB.D (-) m/ z 73.0,0 100.00%
73
5000
43
1 i i n । » 4 » t411 j1 j i i" । Ti r*1
87 7.20 7.40 7.60 7.80 8.00
0- ......... . ............ 38.1 1—— + • i • • » • t ‘ ‘ • i • ‘ ' • * m/z
1 50 55 60 67, 1 103
j 43.0,5 32.06%
m/z-> 10 20 30 40 50 60 70 80 90 100 110
Abundance #292: N-Ethylformamide
30
73
5000 fl » i l pl » » I J 112‘I
58 7.20 7.40 7.60 7.80 8.00
44
m/z 45.05 11.10%
15 I i
.nanlaje 1 1 4 i'I'I'I . । , i ■ ■ ‘ • i 1 1 ■ • i ■ ■ ' ■ i • ■ ■ ■ । ■ 1 ■ 1 i ■ ■
miz-> 10 20 30 40 50 60 70 80 90 100 110
Abundance #62902: 1,3-Dioxolane, 2-methyl
73
[4 » » r p < "" 1 j i j r • j' r 1 • i ■ ■
7.20 7.40 7.60 7.80 8.00
5000 43 m/z 41.00 10.74%
58
27 87
' 1 I 1 1 ‘ rp 1 1, 1’ ' ■ ■ i 1 ■ ■ 1 i ■ • ■ • i ■ ■ ■ ■ i • 1 1 ■ i ■ ■ ■ • i • • ■ ■ I ■ ■ ■ ■ i ■ ■
miz-> 10 20 30 40 50 60 70 80 90 100 110
Abundance #1793: Pentene, 3-methoxy-
73 7.20 7.40 7.60 7.80 8.00
m/z 71.0.0 7.34%
5000
45
. .......... . 33.39, TIIut
55
■ ■ i • ■ • 1 I ■ • 1 ■ i ■ • ■ • i 1 • • 1 ■ • । ■ ■ ■ ■ । • i ' ■ ■ ■ i 1 ‘ 1 11 pni r ■ .
m/z-> 10 20 30 40___ 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00
LBB.D GCMS0103.M Thu Jan 10 13:58:29 2002 Page 1
NYC-WTC_000017132
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