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GCMS blank analysis for sample AD30694, Jan 2002

Machine-extracted title · confidence 100%

Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.

NYC-WTC_000018069–000018092

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018089
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC3101\LBD.D Vial: 26 Acq On 1 Jan 2002 1:10 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

34.38 0.93 ug/1 280961 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4S12 018294-04-7 32 3 3-Is opropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 30 4 Butanoic acid, 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23 Abundance 73 Scan 3195 (34.377 mln): LBD.D (-) m/z 73.00 100.00%

147 5000 221 ----------------------- 281 355

miz-> 43 '" I 1 r 50 117 100 TPr 150 +19 401 429 200 250 300 350 • ‘ I ■ • ' ■ i ■ ■ ‘ ■ i • ‘ 400 450 500 ‘ i ' ‘ 550 34.00 34.20 34.40 34.60 34.80 m/z 147.00 49.53% Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147

5000 ' ' i ' 281 34.00 34.20 34.40 34.60 34.80 45 369 m/z 221.0 28.04% 117 207 249 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #71006: Ethanedicicacid. bis(trimethylsilyl) ester 73

147 34.00 34.20 34.40 34.60 34.80 5000 m/z 281.10 17.09% 45 1 117 । 190 219 1 * I ’ ‘ ■ 1 1 ■ 1 f • । 1 * ■ • 1 ■ ■ ■ ■ । • 1 1 1 1 1 11 1 1 ■ ■ ■ 1 । ■ ■ ‘ ■ । • ■ 1 1 1 • ■ • ■ । ■ ■ miz-> 50 100 150 2(X) 250 300 350 400 450 500 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim AaA4MA-Ap-*— Ye i 73 34.00 34.20 34.40 34.60 34:80 m/z 355.0 15.10% 5000 147 221 231 327 415 [ I I I L 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 34.00 34.20 34'40 34.60 34.80

LBD.D GCMS1126.M Wed Jan 23 09:03:07 2002 Page 15

NYC-WTC_000018089

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NYC-WTC_000018089Source: NYC Law Department, mirrored locally

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