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GCMS blank analysis for sample AD30694, Jan 2002

Machine-extracted title · confidence 100%

Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.

NYC-WTC_000018069–000018092

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC3101\LBD.D Vial: 26 Acq On 1 Jan 2002 1:10 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 1-Monolinoleoylglycerol trimet Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

35.57 1.04 ug/1 194061 Perylene-d12 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1 -Monol inol ylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 Trisiloxi C, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 3 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 38 4 Eth edioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 Abundance Scan 3325 (35.571 mln): LBD.D (-) m/z 73.0.0 100.00% 73

147 5000 221 281 355 35.20 35.40 35.60 35.80 36.00 39 TFT* 95 117 a 100 ' 150 ' 200 1931 , . . 325,1 i . 401 429 250 ' ‘ 360' 350 '460' ‘ ‘ 450 m/z-> __ 50 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 —IIITTTT 35.20 35.40 35.60 35.80 36.00 34 103 m/z 221.05 30.91% 281 । 395 1 ''i 1 1 1 1 i ■ ■ ' irtom 1 l 1 ■ 482 • ■ miz-> 50 100 150 200 250 300 350 400 450 Abundance #74103: Trisiloxane, 1,1.1 5,5.5-hexamethyl-3.3-bis[{trimet 73 147 35.20 35.40 35.60 35.80 36.00 5000 m/z 281.00 17.79% 281 45 369 i । i । * 117..... 207, _ 249 . .... ,, i , m/z-> 50 100 150 '260 250 300 350 400 450 #30949: Mercaptoacetic acid, bis(trimethylsilyl)- AWAAW~/ “YRA Abundance 73 147 35.20 35.40 35.60 35.80 36.00 m/z 355.05 15.33% 5000 221 45 193 — 104 , • ■ 1' ‘ • 1 1 1 1 L । | | | ‘ | | ‘ i r | | ■ i ■ ■ • ■ i ■ m/z~> 50 100 150 200 250 300 350 400 450 35.20 35.40 35.60 35.80 36.00

LBD.D GCMS1126.M Wed Jan 23 09:03:12 2002 Page 16

NYC-WTC_000018090

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NYC-WTC_000018090Source: NYC Law Department, mirrored locally

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