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GCMS analysis results for sample AD29522, Jan 2002

Machine-extracted title · confidence 100%

Quality reviewed GCMS data listing surrogate compounds and retention times from January 3, 2002.

NYC-WTC_000036752–000036778

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036777
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC3101\29522.D Vial: 63 Acq On 3 Jan 2002 3:00 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************** * * ** * * * * * * * * * * * * * * * * * * * Peak Number 20 1-Monolinoleoylglycerol trimet Concentration Rank 19

R.T. EstConc Area Relative to ISTD R.T.

39.58 4.92 ug/1 1879040 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1 -Monolinoleo glycerol trimethylsi 498 C27H54O4Si2 054284-45-6 36 2 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 17 3 Trisiloxane ‘ 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 17 4 3-Isopropox -1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 16 Abundance Scan 3762 (39.585 min): 29522.D (-) m/z 73.00 100.00% 73 147 5000 221 281 355 mI ===== 191 | 249,, .i 327, [ 39.20 39.40 39.60 39.80 40.00 45 105126 401 429 TI ITPT 1 TI । ' । 1| l-l T—I-| I -------- m/z 147.00 64.18% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 147 Tr 5000 34 103 281 A 395, 482 J . 06% 39.20 39.40 39.60 39.80 40.00 m/ Z 221.0 I m/z-> 50 100 150 200 250 300 350 400 450 Abundance #30949: Mercaptoacetic acid, bis(trimett)ylsilyl)- 73 1 147 1 I ■ 1 ■ ■ i ■ TT 39.20 39.40 39.60 39.80 40.00 5000- m/z 281.00 21.76% 221 45 104 193 i- m/z-> 50 100 150 200. 250 300 350 400 450 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet —x - 73 39.20 39.40 39.60 39.80 40.00 147 m/ z 2 07.00 18.81% 5000- 281 45 369 I' i 1 117 _ 297 . 249, — m/z-> 50 100 150 200 250 300 350 400 .450 39.20 39.40 39.60 39.80 40.00

29522.D GCMS1126.M Fri Jan 18 16:49:40 2002 Page 20

NYC-WTC_000036777

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NYC-WTC_000036777Source: NYC Law Department, mirrored locally

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