NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\DEC3101\29522.D Vial: 63
Acq On 3 Jan 2002 3:00 am Operator: 209 GALOS
Sample gems scan 12/7 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
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Peak Number 20 1-Monolinoleoylglycerol trimet Concentration Rank 19
R.T. EstConc Area Relative to ISTD R.T.
39.58 4.92 ug/1 1879040 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1 -Monolinoleo glycerol trimethylsi 498 C27H54O4Si2 054284-45-6 36
2 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 17
3 Trisiloxane ‘ 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 17
4 3-Isopropox -1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 16
Abundance Scan 3762 (39.585 min): 29522.D (-) m/z 73.00 100.00%
73
147
5000 221
281 355 mI =====
191 | 249,, .i 327, [ 39.20 39.40 39.60 39.80 40.00
45 105126 401 429
TI ITPT 1 TI । ' । 1| l-l T—I-| I -------- m/z 147.00 64.18%
m/z-> 50 100 150 200 250 300 350 400 450
Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether
73
207
147 Tr
5000
34 103
281
A 395, 482
J . 06%
39.20 39.40 39.60 39.80 40.00
m/ Z 221.0
I
m/z-> 50 100 150 200 250 300 350 400 450
Abundance #30949: Mercaptoacetic acid, bis(trimett)ylsilyl)-
73
1 147
1 I ■ 1 ■ ■ i ■ TT
39.20 39.40 39.60 39.80 40.00
5000- m/z 281.00 21.76%
221
45
104 193
i-
m/z-> 50 100 150 200. 250 300 350 400 450
Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet —x -
73 39.20 39.40 39.60 39.80 40.00
147 m/ z 2 07.00 18.81%
5000-
281
45 369
I' i 1
117 _ 297 . 249, —
m/z-> 50 100 150 200 250 300 350 400 .450 39.20 39.40 39.60 39.80 40.00
29522.D GCMS1126.M Fri Jan 18 16:49:40 2002 Page 20
NYC-WTC_000036777
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